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What are the grades of sintered filters?

May. 06, 2024

Advances in Filtration Using Sintered Metal Filters

Advances in Filtration Using Sintered Metal Filters

Advances in Filtration Using Sintered Metal Filters

Advances in Filtration Using Sintered Metal Filters

Key takeaways:

  • Sintered metal filters offer high efficiency in particulate removal, with capabilities for backwashing and long service life.

  • These filters are suitable for high-temperature applications and various industrial uses, including chemical and power generation sectors.

  • The design and selection of sintered metal filters depend on their particulate holding capacity and the characteristics of the particles being filtered.

  • They are advantageous for processes requiring high filtration efficiency, durability, and resistance to corrosive environments.

Abstract

Filtration technology utilizing sintered metal media provides excellent performance for separation of particulate matter from either liquid or gas process streams (i.e., liquid/solids and gas/solid separation) in numerous industrial liquid and gas filtration applications. Sintered metal filter media, fabricated from either metal fibers or metal powders into filtration elements, are widely used the in the chemical process, petrochemical and power generation industries. Applications require particulate removal to protect downstream equipment, for product separation, or to meet environmental regulations.

Sintered metal media provide a positive barrier to downstream processes. Sintered metal media have demonstrated high particle efficiency removal, reliable filtration performance, effective backwash capability, and long on-stream service. These filters can provide particulate capture efficiencies of 99.9% or better using either surface or depth media. Operating temperature can be as high as 1000°C, depending on the selection of metal alloy. Along with the filtration efficiency consideration, equally important criteria include corrosion resistance, mechanical strength at service temperature, cake release (blowback cleanability), and long on-stream service life. These issues are critical to achieving successful, cost effective operations.

The life of such filter media (filter operating life) will depend on its particulate holding capacity and corresponding pressure drop. This accumulating cake can be periodically removed using a blowback cycle. The effectiveness of the blowback cycle and filter pressure drop recovery is a critical function of the properties of the accumulating particles in the cake and the filter media. Depth filtration media configured in a polishing filter may be utilized in those applications with light particle loading.

In addition to providing superior filtration in a single pass, clean-in-place backwashable media reducesoperator exposure to process materials and volatile emissions. While applications include high temperature and corrosive environments, any pressure driven filtration process with high operating costs has the potential for improvement using sintered metal filtration technology.

This paper will discuss filter-operating parameters of sintered porous metal media and filtration system design criteria for optimizing performance in a number of chemical process streams.

Introduction

The 21st century brings many economic and environmental challenges to the chemical industry. Major drivers for change include market globalization, demand for improved environmental performance, profitability, productivity and changing workforce requirements. Future competitive advantage in the chemical processing industry will come from patented technology and technical know-how. New economical high yield and high quality processes will characterize much of the industry’s production capacity with improved environmental impact and energy efficiency.

A high percentage of the chemical industry’s products and processes involve solids (particulate) handling. Filtration technology offers a means of reducing solids through mechanical separation via patented filter design and unique systems operation. Filtration can improve product purity, increase throughput capacity, eliminate effluent contamination (minimizing or preventing air and water pollution) and provide protection to valuable equipment downstream of the filter. Advances in filtration technology include the development of continuous processes to replace old batch process technology. Cost savings include less hazardous waste for disposal and labor savings from new technology. Fully automated filter systems can be integrated into plant process controls.

Solids reduction includes the removal of suspended solids from process effluent waste streams and cleaning solvents. The liquid product recovered is valuable for recycle to another chemical feed stream. Waste minimization includes the reduction of hazardous solids materials for recovery or recycle and solids reduction of non-hazardous materials to landfill. Filtration can reduce wastewater feed stream BOD (Biological Oxygen Demand), COD (Chemical Oxygen Demand), TSS (Total Suspended Solids), and TOC (Total Organic Carbon). These are the main parameters for which current emissions are measured with regard to local and international standards.

Filtration Fundamentals

Knowledge of filtration fundamentals is essential to ensure appropriate design of filter media and the optimum selection of appropriate media and filter design for each filtration application. Two main filtration modes can be considered, i.e., depth filtration and surface filtration. In the case of depth filtration, the particles are captured inside the media; while in surface filtration they are retained, as the term explains, at the surface where subsequently a cake of particles is formed.

Surface filtration is primarily a straining (sieving) mechanism where particles larger than the pore size of the filter media are separated at the upstream surface of the filter; their size prevents them from entering or passing through the pore openings. Subsequent particles accumulate as a cake that increases in thickness as more particle-laden fluid is forced into the filter medium. The cake, due to its potentially finer pore structure, may aid in the separation of finer particles than can be achieved by the filter media. However, the cake must exhibit sufficient porosity to permit continued flow through it as filtration proceeds. Processes can be run under constant flow/increasing pressure or constant pressure/decreasing flow. Because most surface filters are not perfectly smooth or have perfectly uniform pore structure, some depth filtration can take place that will affect the life of the filter.

Depth filtration is mainly used in applications where small particle levels have to be separated such as in the protection of downstream equipment against fouling or erosion, protection of catalysts from poisoning and in product purification. The particles penetrate into the media and are subsequently captured within its multiple layer structure. This multiple layer structure prevents premature blocking of the media and increases the capacity to hold dirt and on-stream lifetime. Because the particles are captured within the depth of the media, off-line cleaning will be required. This off-line cleaning can be accomplished with solvents, ultrasonic vibration, pyrolysis, steam cleaning or water back flushing. In addition, the media may be pleated, a configuration that minimizes housing size and cost.

Understanding of the ability of a filter to remove particles from a gas stream passing through it is key to successful filter design and operation. For fluids with low levels of particulate contamination, filtration by capturing the particles within the depth of a porous media is key to achieving high levels of particle efficiency. The structure of sintered metal provides a tortuous path in which particles are captured. Particles capture continues as a cake of deposited particles is formed on the media surface; however, particles are now captured on previously deposited particles. The life of such filters will depend on its dirt holding capacity and corresponding pressure drop. For fluids with high particle loading, the operative filtration mechanism becomes cake filtration. A particle cake is developed over the filter element, which becomes the filtration layer and causes additional pressure drop. The pressure drop increases as the particle loading increases. Once a terminal pressure is reached during the filtration cycle, the filter element is blown back with clean gas and/or washed to dislodge the filter cake. If the pore size in the filter media is chosen correctly, the pressure drop of the media can be recovered to the initial pressure drop. However, if particles become lodged within the porous media during forward flow, and progressively load the media, the pressure drop may not be completely recovered after the cleaning cycle.

Filtration rates are influenced by the properties of the feed particle concentration, viscosity and temperature. The filter operating mode can be constant pressure, constant flow rate, or both with pressure rising and flow rate dropping while filtering. Filtration cycle will be constrained if solids are fast blinding and allowable pressure has been reached, or for cake filtration, if the volume for cake buildup has been filled, even if the allowable pressure drop has not been reached. Permeability is expressed as flow rate against pressure drop. Permeability is influenced by filter type, fluid temperature and solids loading.

Sintered Powder Metal Media

Sintered metal media are manufactured by pressing metal powder into porous sheet or tubes, followed by high temperature sintering. A scanning electron photomicrograph of a typical sintered powder metal media is shown in Figure 1. The combination of powder size, pressing and sintering operation defines the pore size and distribution, strength and permeability of the porous element. Pore size of sintered metal media is determined using ASTM E-128. The media grade designation is equivalent to the mean flow pore, or average pore size of the filter. Sintered metal media are offered in grades 0.1, 0.2, 0.5, 1, 2, 5, 10, 20, 40 and 100. The filtration rating in liquid for media grades 0.2 to 20 is between 1.4 and 35 µm absolute. The filtration rating in gas ranges from 0.1 to 100 µm absolute.

Filter cartridges fabricated from sheet or tubes have an all welded construction. The filter media is designed and engineered with a stable porous matrix, precise bubble point specifications, close thickness tolerances, and uniformity of permeability, which assure reliable filtration performance, effective backwash cleaning and long on-stream service life.

Sintered Metal Fiber Media

Metal fiber filter media consists of very thin (1.5 to 80 μm) metal filaments uniformly laid to form a three-dimensional non-woven structure sintered at the contact points. A scanning electron photomicrograph of a typical sintered metal filter media is shown in Figure 2. These media are explicitly designed for either surface or depth filters. Either single or multi-layered construction are utilized with each layer comprised of potentially different diameter fibers to achieve optimal performance, e.g., pressure drop, filtration efficiency, particle loading capacity, and media strength. The multi-layered material has a graduated design, so the dirt holding capacity is much higher and consequently the life expectancy is longer. The final filter rating is determined by the weight per used layer, the fiber composition of the layer and the combination of several layers. The availability of a high porous structure (up to 85%) offers a very higher permeability and hence a low pressure drop.

The properties of metal fiber filters, fabricated from various metal alloys, for gas filtration applications allow the use in extreme conditions: high temperature, high pressure and corrosive atmospheres. The primary benefits of sintered metal filters are: strength and fracture toughness, high pressure and temperature capabilities, high thermal shock resistance, corrosion resistance, cleanability, all-welded assembly, and long service life.

Fiber metal media have a higher porosity than the powder metal media, thereby resulting in lower pressure drop. For high temperature or corrosive applications, Bekaert has developed fibres in other alloys besides AISI 316L. Inconel® 601 and Fecralloy® are used for high temperatures (up to 560°C and 1000°C respectively) whereas Alloy HR can withstand temperatures up to 600°C and wet corrosive environments.

The inherent toughness of the metal filters provides for continuous, back pulsed operation for extended periods. For high temperature applications, additional criteria such as creep-fatigue interactions, and high temperature corrosion mechanisms need to be addressed. Filters with semi-permanent media are cost effective, since such units lend themselves to minimal downtime, closed and automatic operation with minimal operator intervention, and infrequent maintenance.

The proper selection of filter media with appropriate pore size, strength and corrosion resistance enables long-term filter operation with high efficiency particle retention. The filtration rating in liquid is between 2 and 35 µm absolute. The filtration rating in gas ranges from 0.1 to 10 µm absolute.

Filter Design

The filter design for liquid/solids separation is selected which produces the required filtrate, minimizes backwash or blowdown and maximizes throughput. Three types of filter configurations are described as follows:

1.) Outside-in filtration

Traditional liquid/solids barrier separation occurs on the outer perimeter of a closed-end tubular filter element (LSP). A gas assisted pneumatic hydro-pulse backwash has proven to be the most effective cleaning method for sintered porous metal filters.

2.) Inside-out filtration

Liquid/solid barrier separation occurs on the inside of a closed-end tubular filter element (LSI). LSI backwash modes include: a.) Full shell slurry backwash, b.) Empty shell slurry backwash, c.) Empty shell and empty element wet cake backwash and d.) Empty housing wet cake discharge.

3.) Inside-out Multimode filtration:

Liquid/solids (barrier or crossflow) separation occurs on the inside of open-ended tubular filter element (LSM and LSX). Elements are sealed within two tube sheets, thereby allowing for either top or bottom feed inlet. The LSM filter, with a feed recirculation feature, has proven itself in several continuous loop reactor systems. The downward velocity controls the cake thickness of the catalyst with the lower the velocity resulting in a thicker cake. Filter backwash modes are similar to LSI backwash modes and also includes a bump-and-settle type backwash that allows concentration of solids without draining the filter element or housing. Continuous loop reactor system may not require backwashing.

Scale-ability of the filtration systems allows for accommodating high flow rates and increased solids capacity. Filtration units are suitable for batch or continuous processes. Single housing filter systems are recommended where flow rates allow and flow can be stopped for a few minutes prior to backwash, or if off line periods can be tolerated for maintenance. Two filter dual systems are recommended where continuous flow is required and short periods of off line can be tolerated for maintenance. Three filter systems are recommended for continuous operation even during maintenance periods.

Benchscale and Pilot Testing 

A valid method of evaluating filter performance is through bench scale and pilot testing. Filter testing typically begins with a simple disc feasibility test to qualify media and obtain critical filtration characteristics. Successful feasibility studies usually progresses to more involved testing of pilot equipment. Pilot testing helps develop successful commercial separation practices. While bench scale tests produce reliable indication of filter performance, data obtained in pilot scale testing on a process line will show filter operating parameters with normal process variations. Development programs require direct access to suitable equipment over an extended period. Pilot testing of sintered metal backwashable filters can provide the following information:

  • Verification of filtrate quality;
  • Filter thruput per cycle at various flux rates;
  • Rate of rise in pressure drop vs. thruput;
  • Backwash volume and resulting solids concentration;
  • Scale up data for full scale sizing;
  • Accurate cost estimates;
  • Demonstrate high product value;
  • Reliable operation with high on-line time and low maintenance;
  • Demonstrate new technology at a commercial scale.

In addition to verifying filter performance, pilot testing provides the opportunity for the operating engineer to learn to use the equipment and conduct experiments that optimize filter operation for their particular process. Pilot test trials address significant technical questions and problems prior to full-scale commercialization. The outcome of pilot plant operations verify:

  • Filtration/reaction studies verified at laboratory and pilot plant scale;
  • New technology demonstrated;
  • High volume product consistently recovered;
  • Product separation and recovery optimized;
  • Capacity testing completed;
  • Overall operating efficiency.

Media Selection 

Feasibility Case Study: Catalyst Solids Removal

A typical approach for feasibility testing and media selection is illustrated in the following test case. The objective was to evaluate the filtering characteristics of a new catalyst to support an existing LSI commercial filter installation. Filtration studies were conducted with a 70-mm disc test filter using both Grades 5 and 10 media to compare filter performance. Catalyst particle size distribution (PSD) was measured using a Horiba LA-910 Laser Scattering Particle Size Distribution Analyzer. The size range (based on volume %) was 0.51 to 60 µm with a mean size of 13.4 µm. SEM microscopy at 2000- X magnification verified particle size distribution as shown in Figure 3. Catalyst slurry was filtered once through at a constant rate using Grades 5 and 10 media housed in the 70-mm disc filter housing shown in Figure 4. A particle size distribution comparison of feed and filtrates (Grade 5) sample is shown in Figure 5. Test results indicate that filtration using Grade 5 media resulted with a lower rate of rise pressure than Grade 10 media as indicated in Figure 6. Filtrate turbidity samples were similar. Filtrate from the Grade 5 media measured 2.9 NTU, while filtrate from Grade 10 media measured 2.3 NTU. The 1/8 inch thick filter cake backwashed effectively from the Grade 5 media surface. Some catalyst remained in the porous structure of the Grade 10 media, indicating that catalyst had blocked some of the surface pores.

Test results indicate that Grade 5 media is better suited for filtration of new catalyst sample using the HyPulse LSI filter configuration. Pilot testing at the commercial facility verified results of feasibility study and resulted in purchase of replacement cartridges for an existing filter vessel.

Commercial Applications 

Application 1:

Laboratory disc tests conducted in April 1992 indicate suitability of sintered metal filter for catalyst recovery application. Bench scale pilot filter tests were conducted at the customer’s lab facility to verify filter performance and filtrate quality. In November 1992 pilot testing with continuous catalyst filtration using 2% slurry demonstrated consistent flux rates of 0.2 gpm/ft2. A comparison of filter performance from disc testing through pilot testing is listed in Table 1. Axial velocity through the filter controlled cake thickness. The rate or velocity through the filter was optimized in bench scale testing. Optimal filter performance indicated that the filter could operate at pressures < 10 PSI without backwashing. Tests were conducted over about 1500 hours with no significant change in operating performance. The project gained approval to move to the final stage.

The objective of pilot test development program was to convert isomerization process from batch to continuous. The first commercial plant was scheduled for operation in 1994. The process was started up in July 1994 in accordance with parameters established during the pilot testing. System dynamics experienced during start-up and initial operation exhibited performance similar to the pilot test studies. The filter operated successfully to recover and recycle precious metal catalyst after solvent wash and removal of 10% of the catalyst from the process after each batch. Process liquid is hazardous, however, because the filter system is completely enclosed, solvent could be used to wash and re-slurry catalyst back to the reactor.

The primary (larger) LSM catalyst filter is designed for bulk catalyst filtration and recycle. The filter design offers completely enclosed automated operation with minimal filter cleaning/regeneration. Fresh catalyst is added to each batch. The smaller LSP filter is designed for catalyst removal from the system. After 7 years of operation the filter bundle was replaced during a preventive maintenance schedule. The filtration system continues to operate since its initial installation in 1994.

Application 2:

This catalyst filtration concept was proved in laboratory testing to confirm filter operating parameters and media selection. A development program utilizing pilot testing used a reactor equipped with filtration apparatus capable of separating product from catalyst, whereby the product can be removed from the

reactor while the catalyst is retained, thus permitting the reaction to be run semi-continuously or continuously. Testing utilized the HyPulse® LSM filter design.

By equipping a reactor with a means of maintaining catalyst in the vessel, the reactant can be pumped and the catalyst free product continuously removed. The hydrogenation process stops when the catalyst charge deactivates. The preferred method of filtration was to install a re-circulation loop onto the reactor,

as shown in Figure 7. For an extended batch or continuous process, a larger charge of catalyst is used to ensure sufficiently large commercially viable production quantities. This process allows up to a 50% reduction in total cycle time and an increase in over 65% in the amount of product run as indicated in Table 2.

Application 3:

The first use of sintered metal filters using inside-out (LSI) HyPulse® filtration technology for continuous slurry oil filtration was in 1985. The installation demonstrated the suitability of sintered metal media for high temperature filtration of slurry oil for a carbon fiber development process. The filter operated reliably for many years producing clean oil with solids content of less than 20 ppm and was eventually shut down because of low product demand. Since then, refineries around the world have become aware of the benefits of filtration using sintered metal media for catalyst fines removal in slurry oil service.

Throughout the 1990’s numerous LSI filtration systems have been installed for FCC slurry oil filtration. The largest continuous filtration systems utilizes (3) 66” LSI filters as shown in the schematic in Figure 8. Filtration cycle time ranges from 2 to 16 hours operating at 30 & 60 PSI, respectively in the filtration of 1000 ppm slurry oil. Extended cycle times were obtained by running two filters simultaneously, but staggered in cycle time, with the third being on stand-by for utilization when one of the other filter units is backwashed. The filter design uses a full shell backwash. Efficiency of the recovered product using two filters on line exceeds 99.8%.

Since 1997 there have been many refineries in China have installed LSI filtration systems for catalyst removal in resid fluid catalytic cracking (RFCC) units. A filtration system with (2) 24” LSI filters was installed in a RFCC unit with 1.4 million metric tons (mt) per year capacity and an output of slurry oil of 180 mt/day. The slurry oil has an average 3,000 to 5,000 ppm solids concentration. Cycle time varies from 2 to 8 hours. The filtrate solids content is under 50 ppm. The filter is controlled by local PLC that communicates with refineries distributed control system (DCS) to enable the operator monitor the filtration in the control room. The system is running continuously since then supplying a local company with clean filtrate to produce carbon black.

Application 4:

A process for producing Uranium Dioxide utilizes a HyPulse® gas/solids venturi pulse (GSV) blowback sintered metal filters, as shown in Figure 9, for the recovery of Uranium oxide fines from a process kiln. The sintered metal filters must withstand kiln off-gas stream temperatures of 300°F and be chemically resistant to the gaseous components. The primary risks associated with this conversion are chemical and radiological. The conversion process uses strong acids and alkalis that involve turning uranium oxide into soluble forms, leading to possible inhalation of uranium. In addition, the corrosive chemicals can cause fire or explosion hazards.

Successful field applications and laboratory support provided performance data that resulted in the first commercial filter installation put in service in 1984. The completely enclosed GSV filter operates with 99.999% efficiency with a very low solids load to the filter and infrequent backpulsing. Key operating parameters include controlled approach velocity to the filter, high efficiency, and use of venturi for blowback for continuous operation. Today, one uranium conversion plant continues to operate in the United States using this patented process.

 

 

Application 5:

Cleanable sintered metal fibre filters offer an economical solution to processes with increased demand for higher particulate removal efficiency in extreme conditions. The development of metal fiber filter media such as Bekipor® contributed to an increased quality level through higher filter efficiency and a longer onstream

lifetime. Traditional separation systems such as cyclones, ElectroStatic Precipitators (ESP) and disposable filters are losing their appeal. Figure 10 compares emissions efficiency and relative cost of fiber metal compared to ESP and cyclones.

A highly porous structure, which is a characteristic of a sintered metal fibre medium, offers a high permeability and hence low pressure drop, even at high filtration velocities. This results in a low capital expenditure and low running costs. The cleanability for both on line cleaned surface filtration as for off line cleaned depth filtration is excellent.

This application used Bekiflow® HG for removal of alumina and alumina hydroxide dust having a particle size of 50% < 15 μm. Gas temperatures measured 842 °F. Dust concentration before the filter measured 250-800 mg/Nm³. Gas concentration after filtration was less than 30 mg/Nm³. Maximum pressure drop was 15 mbar. Total surface area of the filter was 830 m2. Fiber metal filters offers limited pressure drop and was tested for guaranteed lifetime of 27,000 operating hours. Customer benefits include less filter surface required, smaller bag house therefore less installation place required.

Summary 

Sintered metal media provides an effective means of filtering to remove particulate whether they are impurities or valuable by-product of a chemical process stream. These media are ideally suited for more demanding applications involving high temperatures, high pressures, and/or corrosive fluids. Chemical

companies are utilizing filtration to minimize waste products at the source rather than at the end of the line of the production process. Filtration improves product quality and protects downstream equipment in the production of chemical based products. Advances in filtration technology include the development of continuous processes to replace old batch process technology. Liquid/solids filtration using conventional leaf filters is messy and hazardous to clean and require extended re-circulation time to obtain clean product. Traditional gas/solids separation systems such as cyclones, ElectroStatic Precipitators (ESP) and disposable filters are being replaced by sintered fiber metal filtration systems.

Sintered metal filters should be operated within the design parameters to prevent premature blinding of the media due to fluctuations in process operations. Use of flow control assures the filter will not be impacted with a high flow excursion. Filter efficiency increases as the filter cake forms. The cake becomes the filter media and the porous media acts as a septum to retain the filter cake. Filter cakes can be effectively washed in-situ and backwashed from the filter housing. A gas assisted pneumatic hydropulse backwash has proven to be the most effective cleaning method for sintered porous metal filters. Sintered metal filters can be fully automated to eliminate operator exposure and lower labor costs while providing reliable, efficient operation.

 

Bekiflow and Bekipor are registered trademarks of Bekaert.

Hypulse is a registered trademark of Mott Corporation.

 

 

FAQs: Sintered Metal Technology

Q: What is sintered metal?

A: Sintered metal refers to a specialized material made by compacting and forming metal powder under heat and pressure, creating a solid, porous structure ideal for filtration and various industrial applications.

Q: How are sintered metal filters manufactured?

A: Sintered metal filters are produced by compacting metal powder in a mold and then heating it to a temperature below the metal’s melting point, causing the particles to bond without liquefying.

Q: What are the main advantages of using sintered metal filters?

A: Sintered metal filters offer high durability, excellent temperature and corrosion resistance, and the ability to withstand harsh environments, making them suitable for challenging industrial applications.

Q: In what industries are sintered metal filters commonly used?

A: Sintered metal filters are widely used across various industries, including pharmaceuticals, food and beverage, chemical processing, and aerospace, for their efficiency in removing particulates from gases and liquids.

 

Types of Sintered Filters and How To Choosing

 

 

1. What are the 4 main filter types?

1. Sintered Metal Filters

These filters are made by fusing together metal particles under heat and pressure. They can be made from different metals and alloys, each having unique properties.

  • Sintered Bronze Filter: Sintered bronze filters are known for their corrosion resistance and are often used in hydraulic systems, pneumatic systems, and other applications where a high degree of filtration is required.

  • Sintered Stainless Steel Filter: This type offers high strength and temperature resistance, and it's often used in demanding environments like chemical processing and food and beverage applications.

  • Sintered Titanium Filter: Titanium offers excellent corrosion resistance and is suitable for use in the pharmaceutical and biotech industries.

  • Sintered Nickel Filter: Nickel sintered filterssintered filters are known for their magnetic properties and are used in various industries including chemical processing and petroleum.

2. Sintered Glass Filter

Sintered glass filters are made by fusing together glass particles. They are widely used in laboratories for filtration tasks and offer a high degree of chemical resistance. They are commonly utilized in applications where precise filtration and minimal interaction with the sample are crucial.

3. Sintered Ceramic Filter

Ceramic filters are made from various ceramic materials and are known for their high-temperature resistance and stability. They are often used in the metal industry for filtering molten metal and in environmental applications to filter air or water.

4. Sintered Plastic Filter

These filters are made by fusing together plastic particles, often polyethylene or polypropylene. Sintered plastic filters are lightweight and corrosion-resistant, and they're typically used in applications where chemical compatibility and cost-effectiveness are key considerations.

In conclusion, the type of sintered filter selected depends on the specific application, considering factors such as temperature, pressure, corrosion resistance, and the nature of the substances being filtered. Different materials offer various advantages and trade-offs, so careful selection is vital to meet the required performance criteria.

 

However, if you're asking about the four main types of filters in general, they are typically categorized by their function rather than the material they are made from. Here's a general overview:

  1. Mechanical Filters: These filters remove particles from air, water, or other fluids through a physical barrier. The sintered filters you mentioned would fall into this category, as they are often used to filter particulates from gases or liquids.

  2. Chemical Filters: These filters use a chemical reaction or absorption process to remove specific substances from a fluid. For example, activated carbon filters are used to remove chlorine and other contaminants from water.

  3. Biological Filters: These filters use living organisms to remove contaminants from water or air. In a fish tank, for example, a biological filter might use bacteria to break down waste products.

  4. Thermal Filters: These filters use heat to separate substances. An example would be an oil filter in a deep fryer that uses heat to separate the oil from other substances.

The sintered filters you mentioned are specific examples of mechanical filters, and they can be made from various materials, including metal, glass, ceramic, and plastic. Different materials will offer different properties, such as resistance to corrosion, strength, and porosity, making them suitable for different applications.

 

 

2. What are sintered filters made of?

Sintered filters are made from a variety of materials, depending on their specific application and required properties. Here's a breakdown of the common materials used:

1. Sintered Metal Filters

  • Bronze: Offers good corrosion resistance.

  • Stainless Steel: Known for high strength and temperature resistance.

  • Titanium: Offers excellent corrosion resistance.

  • Nickel: Used for its magnetic properties.

2. Sintered Glass Filter

  • Glass Particles: Fused together to form a porous structure, often used in laboratory settings for precise filtration.

3. Sintered Ceramic Filter

  • Ceramic Materials: Including alumina, silicon carbide, and other compounds, used for their high-temperature resistance and stability.

4. Sintered Plastic Filter

  • Plastics such as Polyethylene or Polypropylene: These are used for their lightweight and corrosion-resistant properties.

The choice of material is guided by the specific requirements of the application, such as chemical compatibility, temperature resistance, mechanical strength, and cost considerations. Different materials provide different characteristics, making them suitable for various industrial, laboratory, or environmental uses.

 

 

3. What are the different types of sintered filters? Advantage and Disadvantage

Advantages:

  • Durability: Metal filters are robust and can withstand high pressures and temperatures.

  • Variety of Materials: Options like bronze, stainless steel, titanium, and nickel allow for customization based on application needs.

  • Reusable: Can be cleaned and reused, reducing waste.

Disadvantages:

  • Cost: Typically more expensive than plastic or glass filters.

  • Weight: Heavier than other types, which may be a consideration in some applications.

Subtypes:

  • Sintered Bronze, Stainless Steel, Titanium, Nickel: Each metal has specific advantages, such as corrosion resistance for bronze, high strength for stainless steel, and so on.

2. Sintered Glass Filter

Advantages:

  • Chemical Resistance: Resistant to most chemicals, making it suitable for laboratory applications.

  • Precision Filtration: Can achieve fine levels of filtration.

Disadvantages:

  • Fragility: More prone to breaking compared to metal or ceramic filters.

  • Limited Temperature Resistance: Not suitable for very high-temperature applications.

3. Sintered Ceramic Filter

Advantages:

  • High-Temperature Resistance: Suitable for applications involving high temperatures, such as molten metal filtration.

  • Chemical Stability: Resistant to corrosion and chemical attack.

Disadvantages:

  • Brittleness: Can be prone to cracking or breaking if mishandled.

  • Cost: Can be more expensive than plastic filters.

4. Sintered Plastic Filter

Advantages:

  • Lightweight: Easier to handle and install.

  • Corrosion-Resistant: Suitable for applications involving corrosive chemicals.

  • Cost-Effective: Generally more affordable than metal or ceramic filters.

Disadvantages:

  • Lower Temperature Resistance: Not suitable for high-temperature applications.

  • Less Robust: May not withstand high pressures or mechanical stress as well as metal filters.

In conclusion, the selection of a sintered filter depends on various factors, such as the filtration requirements, operating conditions (temperature, pressure, etc.), chemical compatibility, and budget constraints. Understanding the advantages and disadvantages of each type of sintered filter allows for an informed choice that best fits the specific application.

 

 

4. What is a sintered filter used for?

A sintered filter is used in a wide variety of applications across different industries due to its unique properties, including controlled porosity, strength, and chemical resistance. Here's an overview of the common uses for sintered filters:

1. Industrial Filtration

  • Chemical Processing: Removal of impurities from chemicals and liquids.

  • Oil and Gas: Separation of particles from fuels, oils, and gases.

  • Food and Beverage Industry: Ensuring purity and sanitation in processing.

  • Pharmaceutical Manufacturing: Filtering contaminants from pharmaceutical products.

2. Laboratory Applications

  • Analytical Testing: Providing precise filtration for various laboratory tests and experiments.

  • Sample Preparation: Preparing samples by removing unwanted particles or debris.

3. Environmental Protection

  • Water Treatment: Filtering impurities from drinking water or wastewater.

  • Air Filtration: Removing pollutants and particles from the air.

4. Automotive and Transportation

  • Hydraulic Systems: Protecting components by filtering out contaminants in hydraulic fluids.

  • Fuel Filtration: Ensuring clean fuel for efficient engine performance.

5. Medical and Healthcare

  • Medical Devices: Utilized in devices like ventilators and anesthesia machines for clean airflow.

  • Sterilization: Ensuring the purity of gases and liquids in medical applications.

6. Electronics Manufacturing

  • Gas Purification: Providing clean gases used in semiconductor manufacturing.

7. Metal Industry

  • Molten Metal Filtration: Filtering impurities from molten metals during casting processes.

8. Aerospace

  • Fuel and Hydraulic Systems: Ensuring cleanliness and performance in aerospace applications.

The choice of sintered filter, including the material and design, is guided by the specific requirements of the application, such as filtration size, temperature, chemical compatibility, and pressure resistance. Whether it's ensuring the purity of food and water, enhancing industrial processes, or supporting critical healthcare and transportation functions, sintered filters play a vital role in numerous sectors.

 

 

5. How are sintered metal filters made?

Sintered metal filters are made through a process known as sintering, which involves the use of heat and pressure to fuse metal particles into a cohesive, porous structure. Here's a step-by-step explanation of how sintered metal filters are typically made:

1. Material Selection:

  • The process begins by selecting the appropriate metal or metal alloy, such as stainless steel, bronze, titanium, or nickel, depending on the specific application and required properties.

2. Powder Preparation:

  • The selected metal is ground into a fine powder, usually through mechanical milling or atomization.

3. Blending and Mixing:

  • The metal powder may be blended with additives or other materials to achieve specific characteristics, such as enhanced strength or controlled porosity.

4. Shaping:

  • The blended powder is then shaped into the desired form of the filter. This can be done through various methods like pressing, extrusion, or injection molding.

  • In the case of pressing, a mold of the desired filter shape is filled with the powder, and a uniaxial or isostatic press is used to compact the powder into the desired shape.

5. Pre-Sintering (Optional):

  • Some processes may include a pre-sintering step at a lower temperature to remove any organic binders or other volatile substances before the final sintering.

6. Sintering:

  • The shaped part is heated to a temperature below the melting point of the metal but high enough to cause the particles to bond together.

  • This process is usually conducted in a controlled atmosphere to prevent oxidation and contamination.

  • The temperature, pressure, and time are carefully controlled to achieve the desired porosity, strength, and other properties.

7. Post-Processing:

  • After sintering, additional processes like machining, grinding, or heat treatment may be applied to achieve the final dimensions, surface finish, or specific mechanical properties.

  • If required, the filter may be cleaned to remove any residues or impurities from the manufacturing process.

8. Quality Control and Inspection:

  • The final filter is inspected and tested to ensure that it meets the required specifications and standards for the application.

Sintered metal filters are highly customizable, allowing for control over properties like pore size, shape, mechanical strength, and chemical resistance. This makes them suitable for a wide range of demanding filtration applications across various industries.

 

6. What filtration system is most effective?

Determining the "most effective" filtration system depends on the specific requirements of the application, including the type of substance being filtered (e.g., air, water, oil), the desired purity level, operating conditions, budget, and regulatory considerations. Below are some common filtration systems, each with its own set of advantages and suitability for various applications:

1. Reverse Osmosis (RO) Filtration

  • Best For: Water purification, especially for desalination or removal of small contaminants.

  • Advantages: Highly effective at removing salts, ions, and small molecules.

  • Disadvantages: High energy consumption and potential loss of beneficial minerals.

2. Activated Carbon Filtration

  • Best For: Removal of organic compounds, chlorine, and odors in water and air.

  • Advantages: Effective at improving taste and smell, readily available.

  • Disadvantages: Not effective against heavy metals or microorganisms.

3. Ultraviolet (UV) Filtration

  • Best For: Disinfection of water by killing or inactivating microorganisms.

  • Advantages: Chemical-free and highly effective against pathogens.

  • Disadvantages: Does not remove non-living contaminants.

4. High-Efficiency Particulate Air (HEPA) Filtration

  • Best For: Air filtration in homes, healthcare facilities, and cleanrooms.

  • Advantages: Captures 99.97% of particles as small as 0.3 microns.

  • Disadvantages: Does not remove odors or gases.

5. Sintered Filtration

  • Best For: Industrial applications requiring high-temperature resistance and precise filtration.

  • Advantages: Customizable pore sizes, reusable, and suitable for aggressive media.

  • Disadvantages: Potentially higher costs compared to other methods.

6. Ceramic Filtration

  • Best For: Water purification in areas with limited resources.

  • Advantages: Effective at removing bacteria and turbidity, low-cost.

  • Disadvantages: Slower flow rates, may require frequent cleaning.

7. Bag or Cartridge Filtration

  • Best For: General industrial liquid filtration.

  • Advantages: Simple design, easy to maintain, various material options.

  • Disadvantages: Limited filtration capacity, may require frequent replacement.

In conclusion, the most effective filtration system is highly dependent on the specific application, contaminants targeted, operational requirements, and budget considerations. Often, a combination of filtration technologies may be employed to achieve the desired results. Consulting with filtration experts and conducting a proper assessment of the specific needs can guide the selection of the most suitable and effective filtration system.

 

7. What is the type of filter that are commonly used?

There are several types of filters commonly used across various fields and applications. Here are some of the most common types:

  1. Low-Pass Filter: This type of filter allows low-frequency signals to pass through while attenuating high-frequency signals. It's often used to eliminate noise or unwanted high-frequency components from a signal.

  2. High-Pass Filter: High-pass filters allow high-frequency signals to pass while attenuating low-frequency signals. They're used to remove low-frequency noise or DC offset from a signal.

  3. Band-Pass Filter: A band-pass filter allows a certain range of frequencies, called the passband, to pass through while attenuating frequencies outside that range. It's useful for isolating a specific frequency range of interest.

  4. Band-Stop Filter (Notch Filter): Also known as a notch filter, this type of filter attenuates a specific range of frequencies while allowing frequencies outside that range to pass. It's commonly used to eliminate interference from specific frequencies.

  5. Butterworth Filter: This is a type of analog electronic filter that provides a flat frequency response in the passband. It's commonly used in audio applications and signal processing.

  6. Chebyshev Filter: Similar to the Butterworth filter, the Chebyshev filter provides a steeper roll-off between the passband and the stopband, but with some ripple in the passband.

  7. Elliptic Filter (Cauer Filter): This type of filter offers the steepest roll-off between the passband and the stopband but allows for ripple in both regions. It's used when a sharp transition between passband and stopband is needed.

  8. FIR Filter (Finite Impulse Response): FIR filters are digital filters with a finite response duration. They're often used for linear phase filtering and can have both symmetric and asymmetric responses.

  9. IIR Filter (Infinite Impulse Response): IIR filters are digital or analog filters with feedback. They can provide more efficient designs but may introduce phase shifts.

  10. Kalman Filter: A recursive mathematical algorithm used for filtering and predicting future states based on noisy measurements. It's widely used in control systems and sensor fusion applications.

  11. Wiener Filter: A filter used for signal restoration, noise reduction, and image deblurring. It aims to minimize the mean square error between the original and filtered signals.

  12. Median Filter: Used for image processing, this filter replaces each pixel's value with the median value from its neighborhood. It's effective in reducing impulse noise.

These are just a few examples of the many types of filters used in various fields such as signal processing, electronics, telecommunications, image processing, and more. The choice of filter depends on the specific application and the desired characteristics of the filtered output.

 

 

8. ALL Sintered Filter Be Porous ? 

Yes, sintered filters are characterized by their porous nature. Sintering is a process that involves heating and compressing a powdered material, such as metal, ceramic, or plastic, without melting it completely. This results in a solid structure that contains interconnected pores throughout the material.

The porosity of a sintered filter can be carefully controlled during the manufacturing process by adjusting factors such as the particle size of the material, sintering temperature, pressure, and time. The resulting porous structure allows the filter to selectively pass fluids or gases while trapping and removing unwanted particles and contaminants.

The size, shape, and distribution of the pores in a sintered filter can be tailored to meet specific filtration requirements, such as the desired filtration efficiency and flow rate. This makes sintered filters highly versatile and suitable for a wide range of applications, including industrial, chemical, water, and air filtration systems. The ability to control the porosity allows sintered filters to be used for both coarse and fine filtration, depending on the needs of the application.

 

 

9. How to Choose Right Sintered Filters for your Filtration System ?

Choosing the right sintered filters for your filtration system is a critical task that requires careful consideration of various factors. Here's a guide to help you make an informed decision:

1. Identify the Filtration Requirements

  • Contaminants: Determine the type and size of particles or contaminants that need to be filtered.

  • Filtration Efficiency: Decide the level of filtration required (e.g., removing 99% of particles above a certain size).

2. Understand the Operating Conditions

  • Temperature: Choose materials that can withstand the operating temperatures of the system.

  • Pressure: Consider the pressure requirements, as sintered filters must be strong enough to endure the operating pressure.

  • Chemical Compatibility: Select materials that are resistant to any chemicals present in the substances being filtered.

3. Choose the Right Material

  • Sintered Metal Filters: Select from materials like stainless steel, bronze, titanium, or nickel based on the specific needs.

  • Sintered Ceramic or Plastic Filters: Consider these if they meet your temperature, pressure, and chemical resistance requirements.

4. Determine the Pore Size and Structure

  • Pore Size: Choose the pore size based on the smallest particles that need to be filtered.

  • Pore Structure: Consider whether uniform pore sizes or a gradient structure is required for your application.

5. Consider the Flow Rate

  • Evaluate the flow rate requirements of the system and choose a filter with the appropriate permeability to handle the desired flow.

6. Evaluate Cost and Availability

  • Consider the budget constraints and select a filter that offers the required performance at an acceptable cost.

  • Think about the availability and lead time for custom or specialized filters.

7. Compliance and Standards

  • Ensure the selected filter meets any relevant industry standards or regulations specific to your application.

8. Maintenance and Lifecycle Considerations

  • Consider how often the filter will need to be cleaned or replaced and how this fits with maintenance schedules.

  • Think about the expected lifespan of the filter in your specific operating conditions.

9. Consult with Experts or Suppliers

  • If unsure, engage with filtration experts or suppliers who can assist in selecting the right filter for your specific application.

By thoroughly understanding the specific requirements of your system and carefully considering the factors above, you can select the right sintered filter that will deliver the performance, reliability, and efficiency required for your filtration system.

 

Are you looking for the perfect filtration solution tailored to your specific needs?

HENGKO‘s experts specialize in providing top-notch, innovative filtration products designed to meet a wide range of applications.

Don't hesitate to reach out to us with any questions or to discuss your unique requirements.

Contact us today at ka@hengko.com, and let's take the first step towards optimizing your filtration system.

Your satisfaction is our priority, and we're eager to assist you with the best solutions available! 

 

 

Post time: Aug-09-2023

Key takeaways:

  • Sintered metal filters offer high efficiency in particulate removal, with capabilities for backwashing and long service life.

  • These filters are suitable for high-temperature applications and various industrial uses, including chemical and power generation sectors.

  • The design and selection of sintered metal filters depend on their particulate holding capacity and the characteristics of the particles being filtered.

  • They are advantageous for processes requiring high filtration efficiency, durability, and resistance to corrosive environments.

Abstract

Filtration technology utilizing sintered metal media provides excellent performance for separation of particulate matter from either liquid or gas process streams (i.e., liquid/solids and gas/solid separation) in numerous industrial liquid and gas filtration applications. Sintered metal filter media, fabricated from either metal fibers or metal powders into filtration elements, are widely used the in the chemical process, petrochemical and power generation industries. Applications require particulate removal to protect downstream equipment, for product separation, or to meet environmental regulations.

Sintered metal media provide a positive barrier to downstream processes. Sintered metal media have demonstrated high particle efficiency removal, reliable filtration performance, effective backwash capability, and long on-stream service. These filters can provide particulate capture efficiencies of 99.9% or better using either surface or depth media. Operating temperature can be as high as 1000°C, depending on the selection of metal alloy. Along with the filtration efficiency consideration, equally important criteria include corrosion resistance, mechanical strength at service temperature, cake release (blowback cleanability), and long on-stream service life. These issues are critical to achieving successful, cost effective operations.

The life of such filter media (filter operating life) will depend on its particulate holding capacity and corresponding pressure drop. This accumulating cake can be periodically removed using a blowback cycle. The effectiveness of the blowback cycle and filter pressure drop recovery is a critical function of the properties of the accumulating particles in the cake and the filter media. Depth filtration media configured in a polishing filter may be utilized in those applications with light particle loading.

In addition to providing superior filtration in a single pass, clean-in-place backwashable media reducesoperator exposure to process materials and volatile emissions. While applications include high temperature and corrosive environments, any pressure driven filtration process with high operating costs has the potential for improvement using sintered metal filtration technology.

This paper will discuss filter-operating parameters of sintered porous metal media and filtration system design criteria for optimizing performance in a number of chemical process streams.

Introduction

The 21st century brings many economic and environmental challenges to the chemical industry. Major drivers for change include market globalization, demand for improved environmental performance, profitability, productivity and changing workforce requirements. Future competitive advantage in the chemical processing industry will come from patented technology and technical know-how. New economical high yield and high quality processes will characterize much of the industry’s production capacity with improved environmental impact and energy efficiency.

A high percentage of the chemical industry’s products and processes involve solids (particulate) handling. Filtration technology offers a means of reducing solids through mechanical separation via patented filter design and unique systems operation. Filtration can improve product purity, increase throughput capacity, eliminate effluent contamination (minimizing or preventing air and water pollution) and provide protection to valuable equipment downstream of the filter. Advances in filtration technology include the development of continuous processes to replace old batch process technology. Cost savings include less hazardous waste for disposal and labor savings from new technology. Fully automated filter systems can be integrated into plant process controls.

Solids reduction includes the removal of suspended solids from process effluent waste streams and cleaning solvents. The liquid product recovered is valuable for recycle to another chemical feed stream. Waste minimization includes the reduction of hazardous solids materials for recovery or recycle and solids reduction of non-hazardous materials to landfill. Filtration can reduce wastewater feed stream BOD (Biological Oxygen Demand), COD (Chemical Oxygen Demand), TSS (Total Suspended Solids), and TOC (Total Organic Carbon). These are the main parameters for which current emissions are measured with regard to local and international standards.

Filtration Fundamentals

Knowledge of filtration fundamentals is essential to ensure appropriate design of filter media and the optimum selection of appropriate media and filter design for each filtration application. Two main filtration modes can be considered, i.e., depth filtration and surface filtration. In the case of depth filtration, the particles are captured inside the media; while in surface filtration they are retained, as the term explains, at the surface where subsequently a cake of particles is formed.

Surface filtration is primarily a straining (sieving) mechanism where particles larger than the pore size of the filter media are separated at the upstream surface of the filter; their size prevents them from entering or passing through the pore openings. Subsequent particles accumulate as a cake that increases in thickness as more particle-laden fluid is forced into the filter medium. The cake, due to its potentially finer pore structure, may aid in the separation of finer particles than can be achieved by the filter media. However, the cake must exhibit sufficient porosity to permit continued flow through it as filtration proceeds. Processes can be run under constant flow/increasing pressure or constant pressure/decreasing flow. Because most surface filters are not perfectly smooth or have perfectly uniform pore structure, some depth filtration can take place that will affect the life of the filter.

Depth filtration is mainly used in applications where small particle levels have to be separated such as in the protection of downstream equipment against fouling or erosion, protection of catalysts from poisoning and in product purification. The particles penetrate into the media and are subsequently captured within its multiple layer structure. This multiple layer structure prevents premature blocking of the media and increases the capacity to hold dirt and on-stream lifetime. Because the particles are captured within the depth of the media, off-line cleaning will be required. This off-line cleaning can be accomplished with solvents, ultrasonic vibration, pyrolysis, steam cleaning or water back flushing. In addition, the media may be pleated, a configuration that minimizes housing size and cost.

Understanding of the ability of a filter to remove particles from a gas stream passing through it is key to successful filter design and operation. For fluids with low levels of particulate contamination, filtration by capturing the particles within the depth of a porous media is key to achieving high levels of particle efficiency. The structure of sintered metal provides a tortuous path in which particles are captured. Particles capture continues as a cake of deposited particles is formed on the media surface; however, particles are now captured on previously deposited particles. The life of such filters will depend on its dirt holding capacity and corresponding pressure drop. For fluids with high particle loading, the operative filtration mechanism becomes cake filtration. A particle cake is developed over the filter element, which becomes the filtration layer and causes additional pressure drop. The pressure drop increases as the particle loading increases. Once a terminal pressure is reached during the filtration cycle, the filter element is blown back with clean gas and/or washed to dislodge the filter cake. If the pore size in the filter media is chosen correctly, the pressure drop of the media can be recovered to the initial pressure drop. However, if particles become lodged within the porous media during forward flow, and progressively load the media, the pressure drop may not be completely recovered after the cleaning cycle.

Filtration rates are influenced by the properties of the feed particle concentration, viscosity and temperature. The filter operating mode can be constant pressure, constant flow rate, or both with pressure rising and flow rate dropping while filtering. Filtration cycle will be constrained if solids are fast blinding and allowable pressure has been reached, or for cake filtration, if the volume for cake buildup has been filled, even if the allowable pressure drop has not been reached. Permeability is expressed as flow rate against pressure drop. Permeability is influenced by filter type, fluid temperature and solids loading.

Sintered Powder Metal Media

Sintered metal media are manufactured by pressing metal powder into porous sheet or tubes, followed by high temperature sintering. A scanning electron photomicrograph of a typical sintered powder metal media is shown in Figure 1. The combination of powder size, pressing and sintering operation defines the pore size and distribution, strength and permeability of the porous element. Pore size of sintered metal media is determined using ASTM E-128. The media grade designation is equivalent to the mean flow pore, or average pore size of the filter. Sintered metal media are offered in grades 0.1, 0.2, 0.5, 1, 2, 5, 10, 20, 40 and 100. The filtration rating in liquid for media grades 0.2 to 20 is between 1.4 and 35 µm absolute. The filtration rating in gas ranges from 0.1 to 100 µm absolute.

Filter cartridges fabricated from sheet or tubes have an all welded construction. The filter media is designed and engineered with a stable porous matrix, precise bubble point specifications, close thickness tolerances, and uniformity of permeability, which assure reliable filtration performance, effective backwash cleaning and long on-stream service life.

Sintered Metal Fiber Media

Metal fiber filter media consists of very thin (1.5 to 80 μm) metal filaments uniformly laid to form a three-dimensional non-woven structure sintered at the contact points. A scanning electron photomicrograph of a typical sintered metal filter media is shown in Figure 2. These media are explicitly designed for either surface or depth filters. Either single or multi-layered construction are utilized with each layer comprised of potentially different diameter fibers to achieve optimal performance, e.g., pressure drop, filtration efficiency, particle loading capacity, and media strength. The multi-layered material has a graduated design, so the dirt holding capacity is much higher and consequently the life expectancy is longer. The final filter rating is determined by the weight per used layer, the fiber composition of the layer and the combination of several layers. The availability of a high porous structure (up to 85%) offers a very higher permeability and hence a low pressure drop.

The properties of metal fiber filters, fabricated from various metal alloys, for gas filtration applications allow the use in extreme conditions: high temperature, high pressure and corrosive atmospheres. The primary benefits of sintered metal filters are: strength and fracture toughness, high pressure and temperature capabilities, high thermal shock resistance, corrosion resistance, cleanability, all-welded assembly, and long service life.

Fiber metal media have a higher porosity than the powder metal media, thereby resulting in lower pressure drop. For high temperature or corrosive applications, Bekaert has developed fibres in other alloys besides AISI 316L. Inconel® 601 and Fecralloy® are used for high temperatures (up to 560°C and 1000°C respectively) whereas Alloy HR can withstand temperatures up to 600°C and wet corrosive environments.

The inherent toughness of the metal filters provides for continuous, back pulsed operation for extended periods. For high temperature applications, additional criteria such as creep-fatigue interactions, and high temperature corrosion mechanisms need to be addressed. Filters with semi-permanent media are cost effective, since such units lend themselves to minimal downtime, closed and automatic operation with minimal operator intervention, and infrequent maintenance.

The proper selection of filter media with appropriate pore size, strength and corrosion resistance enables long-term filter operation with high efficiency particle retention. The filtration rating in liquid is between 2 and 35 µm absolute. The filtration rating in gas ranges from 0.1 to 10 µm absolute.

Filter Design

The filter design for liquid/solids separation is selected which produces the required filtrate, minimizes backwash or blowdown and maximizes throughput. Three types of filter configurations are described as follows:

1.) Outside-in filtration

Traditional liquid/solids barrier separation occurs on the outer perimeter of a closed-end tubular filter element (LSP). A gas assisted pneumatic hydro-pulse backwash has proven to be the most effective cleaning method for sintered porous metal filters.

2.) Inside-out filtration

Liquid/solid barrier separation occurs on the inside of a closed-end tubular filter element (LSI). LSI backwash modes include: a.) Full shell slurry backwash, b.) Empty shell slurry backwash, c.) Empty shell and empty element wet cake backwash and d.) Empty housing wet cake discharge.

3.) Inside-out Multimode filtration:

Liquid/solids (barrier or crossflow) separation occurs on the inside of open-ended tubular filter element (LSM and LSX). Elements are sealed within two tube sheets, thereby allowing for either top or bottom feed inlet. The LSM filter, with a feed recirculation feature, has proven itself in several continuous loop reactor systems. The downward velocity controls the cake thickness of the catalyst with the lower the velocity resulting in a thicker cake. Filter backwash modes are similar to LSI backwash modes and also includes a bump-and-settle type backwash that allows concentration of solids without draining the filter element or housing. Continuous loop reactor system may not require backwashing.

Scale-ability of the filtration systems allows for accommodating high flow rates and increased solids capacity. Filtration units are suitable for batch or continuous processes. Single housing filter systems are recommended where flow rates allow and flow can be stopped for a few minutes prior to backwash, or if off line periods can be tolerated for maintenance. Two filter dual systems are recommended where continuous flow is required and short periods of off line can be tolerated for maintenance. Three filter systems are recommended for continuous operation even during maintenance periods.

Benchscale and Pilot Testing 

A valid method of evaluating filter performance is through bench scale and pilot testing. Filter testing typically begins with a simple disc feasibility test to qualify media and obtain critical filtration characteristics. Successful feasibility studies usually progresses to more involved testing of pilot equipment. Pilot testing helps develop successful commercial separation practices. While bench scale tests produce reliable indication of filter performance, data obtained in pilot scale testing on a process line will show filter operating parameters with normal process variations. Development programs require direct access to suitable equipment over an extended period. Pilot testing of sintered metal backwashable filters can provide the following information:

  • Verification of filtrate quality;
  • Filter thruput per cycle at various flux rates;
  • Rate of rise in pressure drop vs. thruput;
  • Backwash volume and resulting solids concentration;
  • Scale up data for full scale sizing;
  • Accurate cost estimates;
  • Demonstrate high product value;
  • Reliable operation with high on-line time and low maintenance;
  • Demonstrate new technology at a commercial scale.

In addition to verifying filter performance, pilot testing provides the opportunity for the operating engineer to learn to use the equipment and conduct experiments that optimize filter operation for their particular process. Pilot test trials address significant technical questions and problems prior to full-scale commercialization. The outcome of pilot plant operations verify:

  • Filtration/reaction studies verified at laboratory and pilot plant scale;
  • New technology demonstrated;
  • High volume product consistently recovered;
  • Product separation and recovery optimized;
  • Capacity testing completed;
  • Overall operating efficiency.

Media Selection 

Feasibility Case Study: Catalyst Solids Removal

A typical approach for feasibility testing and media selection is illustrated in the following test case. The objective was to evaluate the filtering characteristics of a new catalyst to support an existing LSI commercial filter installation. Filtration studies were conducted with a 70-mm disc test filter using both Grades 5 and 10 media to compare filter performance. Catalyst particle size distribution (PSD) was measured using a Horiba LA-910 Laser Scattering Particle Size Distribution Analyzer. The size range (based on volume %) was 0.51 to 60 µm with a mean size of 13.4 µm. SEM microscopy at 2000- X magnification verified particle size distribution as shown in Figure 3. Catalyst slurry was filtered once through at a constant rate using Grades 5 and 10 media housed in the 70-mm disc filter housing shown in Figure 4. A particle size distribution comparison of feed and filtrates (Grade 5) sample is shown in Figure 5. Test results indicate that filtration using Grade 5 media resulted with a lower rate of rise pressure than Grade 10 media as indicated in Figure 6. Filtrate turbidity samples were similar. Filtrate from the Grade 5 media measured 2.9 NTU, while filtrate from Grade 10 media measured 2.3 NTU. The 1/8 inch thick filter cake backwashed effectively from the Grade 5 media surface. Some catalyst remained in the porous structure of the Grade 10 media, indicating that catalyst had blocked some of the surface pores.

Test results indicate that Grade 5 media is better suited for filtration of new catalyst sample using the HyPulse LSI filter configuration. Pilot testing at the commercial facility verified results of feasibility study and resulted in purchase of replacement cartridges for an existing filter vessel.

Commercial Applications 

Application 1:

Laboratory disc tests conducted in April 1992 indicate suitability of sintered metal filter for catalyst recovery application. Bench scale pilot filter tests were conducted at the customer’s lab facility to verify filter performance and filtrate quality. In November 1992 pilot testing with continuous catalyst filtration using 2% slurry demonstrated consistent flux rates of 0.2 gpm/ft2. A comparison of filter performance from disc testing through pilot testing is listed in Table 1. Axial velocity through the filter controlled cake thickness. The rate or velocity through the filter was optimized in bench scale testing. Optimal filter performance indicated that the filter could operate at pressures < 10 PSI without backwashing. Tests were conducted over about 1500 hours with no significant change in operating performance. The project gained approval to move to the final stage.

The objective of pilot test development program was to convert isomerization process from batch to continuous. The first commercial plant was scheduled for operation in 1994. The process was started up in July 1994 in accordance with parameters established during the pilot testing. System dynamics experienced during start-up and initial operation exhibited performance similar to the pilot test studies. The filter operated successfully to recover and recycle precious metal catalyst after solvent wash and removal of 10% of the catalyst from the process after each batch. Process liquid is hazardous, however, because the filter system is completely enclosed, solvent could be used to wash and re-slurry catalyst back to the reactor.

The primary (larger) LSM catalyst filter is designed for bulk catalyst filtration and recycle. The filter design offers completely enclosed automated operation with minimal filter cleaning/regeneration. Fresh catalyst is added to each batch. The smaller LSP filter is designed for catalyst removal from the system. After 7 years of operation the filter bundle was replaced during a preventive maintenance schedule. The filtration system continues to operate since its initial installation in 1994.

Application 2:

This catalyst filtration concept was proved in laboratory testing to confirm filter operating parameters and media selection. A development program utilizing pilot testing used a reactor equipped with filtration apparatus capable of separating product from catalyst, whereby the product can be removed from the

reactor while the catalyst is retained, thus permitting the reaction to be run semi-continuously or continuously. Testing utilized the HyPulse® LSM filter design.

By equipping a reactor with a means of maintaining catalyst in the vessel, the reactant can be pumped and the catalyst free product continuously removed. The hydrogenation process stops when the catalyst charge deactivates. The preferred method of filtration was to install a re-circulation loop onto the reactor,

as shown in Figure 7. For an extended batch or continuous process, a larger charge of catalyst is used to ensure sufficiently large commercially viable production quantities. This process allows up to a 50% reduction in total cycle time and an increase in over 65% in the amount of product run as indicated in Table 2.

Application 3:

The first use of sintered metal filters using inside-out (LSI) HyPulse® filtration technology for continuous slurry oil filtration was in 1985. The installation demonstrated the suitability of sintered metal media for high temperature filtration of slurry oil for a carbon fiber development process. The filter operated reliably for many years producing clean oil with solids content of less than 20 ppm and was eventually shut down because of low product demand. Since then, refineries around the world have become aware of the benefits of filtration using sintered metal media for catalyst fines removal in slurry oil service.

Throughout the 1990’s numerous LSI filtration systems have been installed for FCC slurry oil filtration. The largest continuous filtration systems utilizes (3) 66” LSI filters as shown in the schematic in Figure 8. Filtration cycle time ranges from 2 to 16 hours operating at 30 & 60 PSI, respectively in the filtration of 1000 ppm slurry oil. Extended cycle times were obtained by running two filters simultaneously, but staggered in cycle time, with the third being on stand-by for utilization when one of the other filter units is backwashed. The filter design uses a full shell backwash. Efficiency of the recovered product using two filters on line exceeds 99.8%.

Since 1997 there have been many refineries in China have installed LSI filtration systems for catalyst removal in resid fluid catalytic cracking (RFCC) units. A filtration system with (2) 24” LSI filters was installed in a RFCC unit with 1.4 million metric tons (mt) per year capacity and an output of slurry oil of 180 mt/day. The slurry oil has an average 3,000 to 5,000 ppm solids concentration. Cycle time varies from 2 to 8 hours. The filtrate solids content is under 50 ppm. The filter is controlled by local PLC that communicates with refineries distributed control system (DCS) to enable the operator monitor the filtration in the control room. The system is running continuously since then supplying a local company with clean filtrate to produce carbon black.

Application 4:

A process for producing Uranium Dioxide utilizes a HyPulse® gas/solids venturi pulse (GSV) blowback sintered metal filters, as shown in Figure 9, for the recovery of Uranium oxide fines from a process kiln. The sintered metal filters must withstand kiln off-gas stream temperatures of 300°F and be chemically resistant to the gaseous components. The primary risks associated with this conversion are chemical and radiological. The conversion process uses strong acids and alkalis that involve turning uranium oxide into soluble forms, leading to possible inhalation of uranium. In addition, the corrosive chemicals can cause fire or explosion hazards.

Successful field applications and laboratory support provided performance data that resulted in the first commercial filter installation put in service in 1984. The completely enclosed GSV filter operates with 99.999% efficiency with a very low solids load to the filter and infrequent backpulsing. Key operating parameters include controlled approach velocity to the filter, high efficiency, and use of venturi for blowback for continuous operation. Today, one uranium conversion plant continues to operate in the United States using this patented process.

 

 

Application 5:

Cleanable sintered metal fibre filters offer an economical solution to processes with increased demand for higher particulate removal efficiency in extreme conditions. The development of metal fiber filter media such as Bekipor® contributed to an increased quality level through higher filter efficiency and a longer onstream

lifetime. Traditional separation systems such as cyclones, ElectroStatic Precipitators (ESP) and disposable filters are losing their appeal. Figure 10 compares emissions efficiency and relative cost of fiber metal compared to ESP and cyclones.

A highly porous structure, which is a characteristic of a sintered metal fibre medium, offers a high permeability and hence low pressure drop, even at high filtration velocities. This results in a low capital expenditure and low running costs. The cleanability for both on line cleaned surface filtration as for off line cleaned depth filtration is excellent.

This application used Bekiflow® HG for removal of alumina and alumina hydroxide dust having a particle size of 50% < 15 μm. Gas temperatures measured 842 °F. Dust concentration before the filter measured 250-800 mg/Nm³. Gas concentration after filtration was less than 30 mg/Nm³. Maximum pressure drop was 15 mbar. Total surface area of the filter was 830 m2. Fiber metal filters offers limited pressure drop and was tested for guaranteed lifetime of 27,000 operating hours. Customer benefits include less filter surface required, smaller bag house therefore less installation place required.

Summary 

Sintered metal media provides an effective means of filtering to remove particulate whether they are impurities or valuable by-product of a chemical process stream. These media are ideally suited for more demanding applications involving high temperatures, high pressures, and/or corrosive fluids. Chemical

companies are utilizing filtration to minimize waste products at the source rather than at the end of the line of the production process. Filtration improves product quality and protects downstream equipment in the production of chemical based products. Advances in filtration technology include the development of continuous processes to replace old batch process technology. Liquid/solids filtration using conventional leaf filters is messy and hazardous to clean and require extended re-circulation time to obtain clean product. Traditional gas/solids separation systems such as cyclones, ElectroStatic Precipitators (ESP) and disposable filters are being replaced by sintered fiber metal filtration systems.

Sintered metal filters should be operated within the design parameters to prevent premature blinding of the media due to fluctuations in process operations. Use of flow control assures the filter will not be impacted with a high flow excursion. Filter efficiency increases as the filter cake forms. The cake becomes the filter media and the porous media acts as a septum to retain the filter cake. Filter cakes can be effectively washed in-situ and backwashed from the filter housing. A gas assisted pneumatic hydropulse backwash has proven to be the most effective cleaning method for sintered porous metal filters. Sintered metal filters can be fully automated to eliminate operator exposure and lower labor costs while providing reliable, efficient operation.

 

Bekiflow and Bekipor are registered trademarks of Bekaert.

Hypulse is a registered trademark of Mott Corporation.

 

 

FAQs: Sintered Metal Technology

Q: What is sintered metal?

A: Sintered metal refers to a specialized material made by compacting and forming metal powder under heat and pressure, creating a solid, porous structure ideal for filtration and various industrial applications.

Q: How are sintered metal filters manufactured?

A: Sintered metal filters are produced by compacting metal powder in a mold and then heating it to a temperature below the metal’s melting point, causing the particles to bond without liquefying.

Q: What are the main advantages of using sintered metal filters?

A: Sintered metal filters offer high durability, excellent temperature and corrosion resistance, and the ability to withstand harsh environments, making them suitable for challenging industrial applications.

Q: In what industries are sintered metal filters commonly used?

A: Sintered metal filters are widely used across various industries, including pharmaceuticals, food and beverage, chemical processing, and aerospace, for their efficiency in removing particulates from gases and liquids.

 

Types of Sintered Filters and How To Choosing

 

 

1. What are the 4 main filter types?

1. Sintered Metal Filters

These filters are made by fusing together metal particles under heat and pressure. They can be made from different metals and alloys, each having unique properties.

  • Sintered Bronze Filter: Sintered bronze filters are known for their corrosion resistance and are often used in hydraulic systems, pneumatic systems, and other applications where a high degree of filtration is required.

  • Sintered Stainless Steel Filter: This type offers high strength and temperature resistance, and it's often used in demanding environments like chemical processing and food and beverage applications.

  • Sintered Titanium Filter: Titanium offers excellent corrosion resistance and is suitable for use in the pharmaceutical and biotech industries.

  • Sintered Nickel Filter: Nickel sintered filters are known for their magnetic properties and are used in various industries including chemical processing and petroleum.

2. Sintered Glass Filter

Sintered glass filters are made by fusing together glass particles. They are widely used in laboratories for filtration tasks and offer a high degree of chemical resistance. They are commonly utilized in applications where precise filtration and minimal interaction with the sample are crucial.

3. Sintered Ceramic Filter

Ceramic filters are made from various ceramic materials and are known for their high-temperature resistance and stability. They are often used in the metal industry for filtering molten metal and in environmental applications to filter air or water.

4. Sintered Plastic Filter

These filters are made by fusing together plastic particles, often polyethylene or polypropylene. Sintered plastic filters are lightweight and corrosion-resistant, and they're typically used in applications where chemical compatibility and cost-effectiveness are key considerations.

In conclusion, the type of sintered filter selected depends on the specific application, considering factors such as temperature, pressure, corrosion resistance, and the nature of the substances being filtered. Different materials offer various advantages and trade-offs, so careful selection is vital to meet the required performance criteria.

 

However, if you're asking about the four main types of filters in general, they are typically categorized by their function rather than the material they are made from. Here's a general overview:

  1. Mechanical Filters: These filters remove particles from air, water, or other fluids through a physical barrier. The sintered filters you mentioned would fall into this category, as they are often used to filter particulates from gases or liquids.

  2. Chemical Filters: These filters use a chemical reaction or absorption process to remove specific substances from a fluid. For example, activated carbon filters are used to remove chlorine and other contaminants from water.

  3. Biological Filters: These filters use living organisms to remove contaminants from water or air. In a fish tank, for example, a biological filter might use bacteria to break down waste products.

  4. Thermal Filters: These filters use heat to separate substances. An example would be an oil filter in a deep fryer that uses heat to separate the oil from other substances.

The sintered filters you mentioned are specific examples of mechanical filters, and they can be made from various materials, including metal, glass, ceramic, and plastic. Different materials will offer different properties, such as resistance to corrosion, strength, and porosity, making them suitable for different applications.

 

 

2. What are sintered filters made of?

Sintered filters are made from a variety of materials, depending on their specific application and required properties. Here's a breakdown of the common materials used:

1. Sintered Metal Filters

  • Bronze: Offers good corrosion resistance.

  • Stainless Steel: Known for high strength and temperature resistance.

  • Titanium: Offers excellent corrosion resistance.

  • Nickel: Used for its magnetic properties.

2. Sintered Glass Filter

  • Glass Particles: Fused together to form a porous structure, often used in laboratory settings for precise filtration.

3. Sintered Ceramic Filter

  • Ceramic Materials: Including alumina, silicon carbide, and other compounds, used for their high-temperature resistance and stability.

4. Sintered Plastic Filter

  • Plastics such as Polyethylene or Polypropylene: These are used for their lightweight and corrosion-resistant properties.

The choice of material is guided by the specific requirements of the application, such as chemical compatibility, temperature resistance, mechanical strength, and cost considerations. Different materials provide different characteristics, making them suitable for various industrial, laboratory, or environmental uses.

 

 

3. What are the different types of sintered filters? Advantage and Disadvantage

Advantages:

  • Durability: Metal filters are robust and can withstand high pressures and temperatures.

  • Variety of Materials: Options like bronze, stainless steel, titanium, and nickel allow for customization based on application needs.

  • Reusable: Can be cleaned and reused, reducing waste.

Disadvantages:

  • Cost: Typically more expensive than plastic or glass filters.

  • Weight: Heavier than other types, which may be a consideration in some applications.

Subtypes:

  • Sintered Bronze, Stainless Steel, Titanium, Nickel: Each metal has specific advantages, such as corrosion resistance for bronze, high strength for stainless steel, and so on.

2. Sintered Glass Filter

Advantages:

  • Chemical Resistance: Resistant to most chemicals, making it suitable for laboratory applications.

  • Precision Filtration: Can achieve fine levels of filtration.

Disadvantages:

  • Fragility: More prone to breaking compared to metal or ceramic filters.

  • Limited Temperature Resistance: Not suitable for very high-temperature applications.

3. Sintered Ceramic Filter

Advantages:

  • High-Temperature Resistance: Suitable for applications involving high temperatures, such as molten metal filtration.

  • Chemical Stability: Resistant to corrosion and chemical attack.

Disadvantages:

  • Brittleness: Can be prone to cracking or breaking if mishandled.

  • Cost: Can be more expensive than plastic filters.

4. Sintered Plastic Filter

Advantages:

Disadvantages:

  • Lower Temperature Resistance: Not suitable for high-temperature applications.

  • Less Robust: May not withstand high pressures or mechanical stress as well as metal filters.

In conclusion, the selection of a sintered filter depends on various factors, such as the filtration requirements, operating conditions (temperature, pressure, etc.), chemical compatibility, and budget constraints. Understanding the advantages and disadvantages of each type of sintered filter allows for an informed choice that best fits the specific application.

 

 

4. What is a sintered filter used for?

A sintered filter is used in a wide variety of applications across different industries due to its unique properties, including controlled porosity, strength, and chemical resistance. Here's an overview of the common uses for sintered filters:

1. Industrial Filtration

  • Chemical Processing: Removal of impurities from chemicals and liquids.

  • Oil and Gas: Separation of particles from fuels, oils, and gases.

  • Food and Beverage Industry: Ensuring purity and sanitation in processing.

  • Pharmaceutical Manufacturing: Filtering contaminants from pharmaceutical products.

2. Laboratory Applications

  • Analytical Testing: Providing precise filtration for various laboratory tests and experiments.

  • Sample Preparation: Preparing samples by removing unwanted particles or debris.

3. Environmental Protection

  • Water Treatment: Filtering impurities from drinking water or wastewater.

  • Air Filtration: Removing pollutants and particles from the air.

4. Automotive and Transportation

  • Hydraulic Systems: Protecting components by filtering out contaminants in hydraulic fluids.

  • Fuel Filtration: Ensuring clean fuel for efficient engine performance.

5. Medical and Healthcare

  • Medical Devices: Utilized in devices like ventilators and anesthesia machines for clean airflow.

  • Sterilization: Ensuring the purity of gases and liquids in medical applications.

6. Electronics Manufacturing

  • Gas Purification: Providing clean gases used in semiconductor manufacturing.

7. Metal Industry

  • Molten Metal Filtration: Filtering impurities from molten metals during casting processes.

8. Aerospace

  • Fuel and Hydraulic Systems: Ensuring cleanliness and performance in aerospace applications.

The choice of sintered filter, including the material and design, is guided by the specific requirements of the application, such as filtration size, temperature, chemical compatibility, and pressure resistance. Whether it's ensuring the purity of food and water, enhancing industrial processes, or supporting critical healthcare and transportation functions, sintered filters play a vital role in numerous sectors.

 

 

5. How are sintered metal filters made?

Sintered metal filters are made through a process known as sintering, which involves the use of heat and pressure to fuse metal particles into a cohesive, porous structure. Here's a step-by-step explanation of how sintered metal filters are typically made:

1. Material Selection:

  • The process begins by selecting the appropriate metal or metal alloy, such as stainless steel, bronze, titanium, or nickel, depending on the specific application and required properties.

2. Powder Preparation:

  • The selected metal is ground into a fine powder, usually through mechanical milling or atomization.

3. Blending and Mixing:

  • The metal powder may be blended with additives or other materials to achieve specific characteristics, such as enhanced strength or controlled porosity.

4. Shaping:

  • The blended powder is then shaped into the desired form of the filter. This can be done through various methods like pressing, extrusion, or injection molding.

  • In the case of pressing, a mold of the desired filter shape is filled with the powder, and a uniaxial or isostatic press is used to compact the powder into the desired shape.

5. Pre-Sintering (Optional):

  • Some processes may include a pre-sintering step at a lower temperature to remove any organic binders or other volatile substances before the final sintering.

6. Sintering:

  • The shaped part is heated to a temperature below the melting point of the metal but high enough to cause the particles to bond together.

  • This process is usually conducted in a controlled atmosphere to prevent oxidation and contamination.

  • The temperature, pressure, and time are carefully controlled to achieve the desired porosity, strength, and other properties.

7. Post-Processing:

  • After sintering, additional processes like machining, grinding, or heat treatment may be applied to achieve the final dimensions, surface finish, or specific mechanical properties.

  • If required, the filter may be cleaned to remove any residues or impurities from the manufacturing process.

8. Quality Control and Inspection:

  • The final filter is inspected and tested to ensure that it meets the required specifications and standards for the application.

Sintered metal filters are highly customizable, allowing for control over properties like pore size, shape, mechanical strength, and chemical resistance. This makes them suitable for a wide range of demanding filtration applications across various industries.

 

6. What filtration system is most effective?

Determining the "most effective" filtration system depends on the specific requirements of the application, including the type of substance being filtered (e.g., air, water, oil), the desired purity level, operating conditions, budget, and regulatory considerations. Below are some common filtration systems, each with its own set of advantages and suitability for various applications:

1. Reverse Osmosis (RO) Filtration

  • Best For: Water purification, especially for desalination or removal of small contaminants.

  • Advantages: Highly effective at removing salts, ions, and small molecules.

  • Disadvantages: High energy consumption and potential loss of beneficial minerals.

2. Activated Carbon Filtration

  • Best For: Removal of organic compounds, chlorine, and odors in water and air.

  • Advantages: Effective at improving taste and smell, readily available.

  • Disadvantages: Not effective against heavy metals or microorganisms.

3. Ultraviolet (UV) Filtration

  • Best For: Disinfection of water by killing or inactivating microorganisms.

  • Advantages: Chemical-free and highly effective against pathogens.

  • Disadvantages: Does not remove non-living contaminants.

4. High-Efficiency Particulate Air (HEPA) Filtration

  • Best For: Air filtration in homes, healthcare facilities, and cleanrooms.

  • Advantages: Captures 99.97% of particles as small as 0.3 microns.

  • Disadvantages: Does not remove odors or gases.

5. Sintered Filtration

  • Best For: Industrial applications requiring high-temperature resistance and precise filtration.

  • Advantages: Customizable pore sizes, reusable, and suitable for aggressive media.

  • Disadvantages: Potentially higher costs compared to other methods.

6. Ceramic Filtration

  • Best For: Water purification in areas with limited resources.

  • Advantages: Effective at removing bacteria and turbidity, low-cost.

  • Disadvantages: Slower flow rates, may require frequent cleaning.

7. Bag or Cartridge Filtration

  • Best For: General industrial liquid filtration.

  • Advantages: Simple design, easy to maintain, various material options.

  • Disadvantages: Limited filtration capacity, may require frequent replacement.

In conclusion, the most effective filtration system is highly dependent on the specific application, contaminants targeted, operational requirements, and budget considerations. Often, a combination of filtration technologies may be employed to achieve the desired results. Consulting with filtration experts and conducting a proper assessment of the specific needs can guide the selection of the most suitable and effective filtration system.

 

7. What is the type of filter that are commonly used?

There are several types of filters commonly used across various fields and applications. Here are some of the most common types:

  1. Low-Pass Filter: This type of filter allows low-frequency signals to pass through while attenuating high-frequency signals. It's often used to eliminate noise or unwanted high-frequency components from a signal.

  2. High-Pass Filter: High-pass filters allow high-frequency signals to pass while attenuating low-frequency signals. They're used to remove low-frequency noise or DC offset from a signal.

  3. Band-Pass Filter: A band-pass filter allows a certain range of frequencies, called the passband, to pass through while attenuating frequencies outside that range. It's useful for isolating a specific frequency range of interest.

  4. Band-Stop Filter (Notch Filter): Also known as a notch filter, this type of filter attenuates a specific range of frequencies while allowing frequencies outside that range to pass. It's commonly used to eliminate interference from specific frequencies.

  5. Butterworth Filter: This is a type of analog electronic filter that provides a flat frequency response in the passband. It's commonly used in audio applications and signal processing.

  6. Chebyshev Filter: Similar to the Butterworth filter, the Chebyshev filter provides a steeper roll-off between the passband and the stopband, but with some ripple in the passband.

  7. Elliptic Filter (Cauer Filter): This type of filter offers the steepest roll-off between the passband and the stopband but allows for ripple in both regions. It's used when a sharp transition between passband and stopband is needed.

  8. FIR Filter (Finite Impulse Response): FIR filters are digital filters with a finite response duration. They're often used for linear phase filtering and can have both symmetric and asymmetric responses.

  9. IIR Filter (Infinite Impulse Response): IIR filters are digital or analog filters with feedback. They can provide more efficient designs but may introduce phase shifts.

  10. Kalman Filter: A recursive mathematical algorithm used for filtering and predicting future states based on noisy measurements. It's widely used in control systems and sensor fusion applications.

  11. Wiener Filter: A filter used for signal restoration, noise reduction, and image deblurring. It aims to minimize the mean square error between the original and filtered signals.

  12. Median Filter: Used for image processing, this filter replaces each pixel's value with the median value from its neighborhood. It's effective in reducing impulse noise.

These are just a few examples of the many types of filters used in various fields such as signal processing, electronics, telecommunications, image processing, and more. The choice of filter depends on the specific application and the desired characteristics of the filtered output.

 

 

8. ALL Sintered Filter Be Porous ? 

Yes, sintered filters are characterized by their porous nature. Sintering is a process that involves heating and compressing a powdered material, such as metal, ceramic, or plastic, without melting it completely. This results in a solid structure that contains interconnected pores throughout the material.

The porosity of a sintered filter can be carefully controlled during the manufacturing process by adjusting factors such as the particle size of the material, sintering temperature, pressure, and time. The resulting porous structure allows the filter to selectively pass fluids or gases while trapping and removing unwanted particles and contaminants.

The size, shape, and distribution of the pores in a sintered filter can be tailored to meet specific filtration requirements, such as the desired filtration efficiency and flow rate. This makes sintered filters highly versatile and suitable for a wide range of applications, including industrial, chemical, water, and air filtration systems. The ability to control the porosity allows sintered filters to be used for both coarse and fine filtration, depending on the needs of the application.

 

 

9. How to Choose Right Sintered Filters for your Filtration System ?

Choosing the right sintered filters for your filtration system is a critical task that requires careful consideration of various factors. Here's a guide to help you make an informed decision:

1. Identify the Filtration Requirements

  • Contaminants: Determine the type and size of particles or contaminants that need to be filtered.

  • Filtration Efficiency: Decide the level of filtration required (e.g., removing 99% of particles above a certain size).

2. Understand the Operating Conditions

  • Temperature: Choose materials that can withstand the operating temperatures of the system.

  • Pressure: Consider the pressure requirements, as sintered filters must be strong enough to endure the operating pressure.

  • Chemical Compatibility: Select materials that are resistant to any chemicals present in the substances being filtered.

3. Choose the Right Material

  • Sintered Metal Filters: Select from materials like stainless steel, bronze, titanium, or nickel based on the specific needs.

  • Sintered Ceramic or Plastic Filters: Consider these if they meet your temperature, pressure, and chemical resistance requirements.

4. Determine the Pore Size and Structure

  • Pore Size: Choose the pore size based on the smallest particles that need to be filtered.

  • Pore Structure: Consider whether uniform pore sizes or a gradient structure is required for your application.

5. Consider the Flow Rate

  • Evaluate the flow rate requirements of the system and choose a filter with the appropriate permeability to handle the desired flow.

6. Evaluate Cost and Availability

  • Consider the budget constraints and select a filter that offers the required performance at an acceptable cost.

  • Think about the availability and lead time for custom or specialized filters.

7. Compliance and Standards

  • Ensure the selected filter meets any relevant industry standards or regulations specific to your application.

8. Maintenance and Lifecycle Considerations

  • Consider how often the filter will need to be cleaned or replaced and how this fits with maintenance schedules.

  • Think about the expected lifespan of the filter in your specific operating conditions.

9. Consult with Experts or Suppliers

  • If unsure, engage with filtration experts or suppliers who can assist in selecting the right filter for your specific application.

By thoroughly understanding the specific requirements of your system and carefully considering the factors above, you can select the right sintered filter that will deliver the performance, reliability, and efficiency required for your filtration system.

 

Are you looking for the perfect filtration solution tailored to your specific needs?

HENGKO‘s experts specialize in providing top-notch, innovative filtration products designed to meet a wide range of applications.

Don't hesitate to reach out to us with any questions or to discuss your unique requirements.

Contact us today at ka@hengko.com, and let's take the first step towards optimizing your filtration system.

Your satisfaction is our priority, and we're eager to assist you with the best solutions available! 

 

 

Advances in Filtration Using Sintered Metal Filters

Advances in Filtration Using Sintered Metal Filters

Key takeaways:

  • Sintered metal filters offer high efficiency in particulate removal, with capabilities for backwashing and long service life.

  • These filters are suitable for high-temperature applications and various industrial uses, including chemical and power generation sectors.

  • The design and selection of sintered metal filters depend on their particulate holding capacity and the characteristics of the particles being filtered.

  • They are advantageous for processes requiring high filtration efficiency, durability, and resistance to corrosive environments.

Abstract

Filtration technology utilizing sintered metal media provides excellent performance for separation of particulate matter from either liquid or gas process streams (i.e., liquid/solids and gas/solid separation) in numerous industrial liquid and gas filtration applications. Sintered metal filter media, fabricated from either metal fibers or metal powders into filtration elements, are widely used the in the chemical process, petrochemical and power generation industries. Applications require particulate removal to protect downstream equipment, for product separation, or to meet environmental regulations.

Sintered metal media provide a positive barrier to downstream processes. Sintered metal media have demonstrated high particle efficiency removal, reliable filtration performance, effective backwash capability, and long on-stream service. These filters can provide particulate capture efficiencies of 99.9% or better using either surface or depth media. Operating temperature can be as high as 1000°C, depending on the selection of metal alloy. Along with the filtration efficiency consideration, equally important criteria include corrosion resistance, mechanical strength at service temperature, cake release (blowback cleanability), and long on-stream service life. These issues are critical to achieving successful, cost effective operations.

The life of such filter media (filter operating life) will depend on its particulate holding capacity and corresponding pressure drop. This accumulating cake can be periodically removed using a blowback cycle. The effectiveness of the blowback cycle and filter pressure drop recovery is a critical function of the properties of the accumulating particles in the cake and the filter media. Depth filtration media configured in a polishing filter may be utilized in those applications with light particle loading.

In addition to providing superior filtration in a single pass, clean-in-place backwashable media reducesoperator exposure to process materials and volatile emissions. While applications include high temperature and corrosive environments, any pressure driven filtration process with high operating costs has the potential for improvement using sintered metal filtration technology.

This paper will discuss filter-operating parameters of sintered porous metal media and filtration system design criteria for optimizing performance in a number of chemical process streams.

Introduction

The 21st century brings many economic and environmental challenges to the chemical industry. Major drivers for change include market globalization, demand for improved environmental performance, profitability, productivity and changing workforce requirements. Future competitive advantage in the chemical processing industry will come from patented technology and technical know-how. New economical high yield and high quality processes will characterize much of the industry’s production capacity with improved environmental impact and energy efficiency.

A high percentage of the chemical industry’s products and processes involve solids (particulate) handling. Filtration technology offers a means of reducing solids through mechanical separation via patented filter design and unique systems operation. Filtration can improve product purity, increase throughput capacity, eliminate effluent contamination (minimizing or preventing air and water pollution) and provide protection to valuable equipment downstream of the filter. Advances in filtration technology include the development of continuous processes to replace old batch process technology. Cost savings include less hazardous waste for disposal and labor savings from new technology. Fully automated filter systems can be integrated into plant process controls.

Solids reduction includes the removal of suspended solids from process effluent waste streams and cleaning solvents. The liquid product recovered is valuable for recycle to another chemical feed stream. Waste minimization includes the reduction of hazardous solids materials for recovery or recycle and solids reduction of non-hazardous materials to landfill. Filtration can reduce wastewater feed stream BOD (Biological Oxygen Demand), COD (Chemical Oxygen Demand), TSS (Total Suspended Solids), and TOC (Total Organic Carbon). These are the main parameters for which current emissions are measured with regard to local and international standards.

Filtration Fundamentals

Knowledge of filtration fundamentals is essential to ensure appropriate design of filter media and the optimum selection of appropriate media and filter design for each filtration application. Two main filtration modes can be considered, i.e., depth filtration and surface filtration. In the case of depth filtration, the particles are captured inside the media; while in surface filtration they are retained, as the term explains, at the surface where subsequently a cake of particles is formed.

Surface filtration is primarily a straining (sieving) mechanism where particles larger than the pore size of the filter media are separated at the upstream surface of the filter; their size prevents them from entering or passing through the pore openings. Subsequent particles accumulate as a cake that increases in thickness as more particle-laden fluid is forced into the filter medium. The cake, due to its potentially finer pore structure, may aid in the separation of finer particles than can be achieved by the filter media. However, the cake must exhibit sufficient porosity to permit continued flow through it as filtration proceeds. Processes can be run under constant flow/increasing pressure or constant pressure/decreasing flow. Because most surface filters are not perfectly smooth or have perfectly uniform pore structure, some depth filtration can take place that will affect the life of the filter.

Depth filtration is mainly used in applications where small particle levels have to be separated such as in the protection of downstream equipment against fouling or erosion, protection of catalysts from poisoning and in product purification. The particles penetrate into the media and are subsequently captured within its multiple layer structure. This multiple layer structure prevents premature blocking of the media and increases the capacity to hold dirt and on-stream lifetime. Because the particles are captured within the depth of the media, off-line cleaning will be required. This off-line cleaning can be accomplished with solvents, ultrasonic vibration, pyrolysis, steam cleaning or water back flushing. In addition, the media may be pleated, a configuration that minimizes housing size and cost.

Understanding of the ability of a filter to remove particles from a gas stream passing through it is key to successful filter design and operation. For fluids with low levels of particulate contamination, filtration by capturing the particles within the depth of a porous media is key to achieving high levels of particle efficiency. The structure of sintered metal provides a tortuous path in which particles are captured. Particles capture continues as a cake of deposited particles is formed on the media surface; however, particles are now captured on previously deposited particles. The life of such filters will depend on its dirt holding capacity and corresponding pressure drop. For fluids with high particle loading, the operative filtration mechanism becomes cake filtration. A particle cake is developed over the filter element, which becomes the filtration layer and causes additional pressure drop. The pressure drop increases as the particle loading increases. Once a terminal pressure is reached during the filtration cycle, the filter element is blown back with clean gas and/or washed to dislodge the filter cake. If the pore size in the filter media is chosen correctly, the pressure drop of the media can be recovered to the initial pressure drop. However, if particles become lodged within the porous media during forward flow, and progressively load the media, the pressure drop may not be completely recovered after the cleaning cycle.

Filtration rates are influenced by the properties of the feed particle concentration, viscosity and temperature. The filter operating mode can be constant pressure, constant flow rate, or both with pressure rising and flow rate dropping while filtering. Filtration cycle will be constrained if solids are fast blinding and allowable pressure has been reached, or for cake filtration, if the volume for cake buildup has been filled, even if the allowable pressure drop has not been reached. Permeability is expressed as flow rate against pressure drop. Permeability is influenced by filter type, fluid temperature and solids loading.

Sintered Powder Metal Media

Sintered metal media are manufactured by pressing metal powder into porous sheet or tubes, followed by high temperature sintering. A scanning electron photomicrograph of a typical sintered powder metal media is shown in Figure 1. The combination of powder size, pressing and sintering operation defines the pore size and distribution, strength and permeability of the porous element. Pore size of sintered metal media is determined using ASTM E-128. The media grade designation is equivalent to the mean flow pore, or average pore size of the filter. Sintered metal media are offered in grades 0.1, 0.2, 0.5, 1, 2, 5, 10, 20, 40 and 100. The filtration rating in liquid for media grades 0.2 to 20 is between 1.4 and 35 µm absolute. The filtration rating in gas ranges from 0.1 to 100 µm absolute.

Filter cartridges fabricated from sheet or tubes have an all welded construction. The filter media is designed and engineered with a stable porous matrix, precise bubble point specifications, close thickness tolerances, and uniformity of permeability, which assure reliable filtration performance, effective backwash cleaning and long on-stream service life.

Sintered Metal Fiber Media

Metal fiber filter media consists of very thin (1.5 to 80 μm) metal filaments uniformly laid to form a three-dimensional non-woven structure sintered at the contact points. A scanning electron photomicrograph of a typical sintered metal filter media is shown in Figure 2. These media are explicitly designed for either surface or depth filters. Either single or multi-layered construction are utilized with each layer comprised of potentially different diameter fibers to achieve optimal performance, e.g., pressure drop, filtration efficiency, particle loading capacity, and media strength. The multi-layered material has a graduated design, so the dirt holding capacity is much higher and consequently the life expectancy is longer. The final filter rating is determined by the weight per used layer, the fiber composition of the layer and the combination of several layers. The availability of a high porous structure (up to 85%) offers a very higher permeability and hence a low pressure drop.

The properties of metal fiber filters, fabricated from various metal alloys, for gas filtration applications allow the use in extreme conditions: high temperature, high pressure and corrosive atmospheres. The primary benefits of sintered metal filters are: strength and fracture toughness, high pressure and temperature capabilities, high thermal shock resistance, corrosion resistance, cleanability, all-welded assembly, and long service life.

Fiber metal media have a higher porosity than the powder metal media, thereby resulting in lower pressure drop. For high temperature or corrosive applications, Bekaert has developed fibres in other alloys besides AISI 316L. Inconel® 601 and Fecralloy® are used for high temperatures (up to 560°C and 1000°C respectively) whereas Alloy HR can withstand temperatures up to 600°C and wet corrosive environments.

The inherent toughness of the metal filters provides for continuous, back pulsed operation for extended periods. For high temperature applications, additional criteria such as creep-fatigue interactions, and high temperature corrosion mechanisms need to be addressed. Filters with semi-permanent media are cost effective, since such units lend themselves to minimal downtime, closed and automatic operation with minimal operator intervention, and infrequent maintenance.

The proper selection of filter media with appropriate pore size, strength and corrosion resistance enables long-term filter operation with high efficiency particle retention. The filtration rating in liquid is between 2 and 35 µm absolute. The filtration rating in gas ranges from 0.1 to 10 µm absolute.

Filter Design

The filter design for liquid/solids separation is selected which produces the required filtrate, minimizes backwash or blowdown and maximizes throughput. Three types of filter configurations are described as follows:

1.) Outside-in filtration

Traditional liquid/solids barrier separation occurs on the outer perimeter of a closed-end tubular filter element (LSP). A gas assisted pneumatic hydro-pulse backwash has proven to be the most effective cleaning method for sintered porous metal filters.

2.) Inside-out filtration

Liquid/solid barrier separation occurs on the inside of a closed-end tubular filter element (LSI). LSI backwash modes include: a.) Full shell slurry backwash, b.) Empty shell slurry backwash, c.) Empty shell and empty element wet cake backwash and d.) Empty housing wet cake discharge.

3.) Inside-out Multimode filtration:

Liquid/solids (barrier or crossflow) separation occurs on the inside of open-ended tubular filter element (LSM and LSX). Elements are sealed within two tube sheets, thereby allowing for either top or bottom feed inlet. The LSM filter, with a feed recirculation feature, has proven itself in several continuous loop reactor systems. The downward velocity controls the cake thickness of the catalyst with the lower the velocity resulting in a thicker cake. Filter backwash modes are similar to LSI backwash modes and also includes a bump-and-settle type backwash that allows concentration of solids without draining the filter element or housing. Continuous loop reactor system may not require backwashing.

Scale-ability of the filtration systems allows for accommodating high flow rates and increased solids capacity. Filtration units are suitable for batch or continuous processes. Single housing filter systems are recommended where flow rates allow and flow can be stopped for a few minutes prior to backwash, or if off line periods can be tolerated for maintenance. Two filter dual systems are recommended where continuous flow is required and short periods of off line can be tolerated for maintenance. Three filter systems are recommended for continuous operation even during maintenance periods.

Benchscale and Pilot Testing 

A valid method of evaluating filter performance is through bench scale and pilot testing. Filter testing typically begins with a simple disc feasibility test to qualify media and obtain critical filtration characteristics. Successful feasibility studies usually progresses to more involved testing of pilot equipment. Pilot testing helps develop successful commercial separation practices. While bench scale tests produce reliable indication of filter performance, data obtained in pilot scale testing on a process line will show filter operating parameters with normal process variations. Development programs require direct access to suitable equipment over an extended period. Pilot testing of sintered metal backwashable filters can provide the following information:

  • Verification of filtrate quality;
  • Filter thruput per cycle at various flux rates;
  • Rate of rise in pressure drop vs. thruput;
  • Backwash volume and resulting solids concentration;
  • Scale up data for full scale sizing;
  • Accurate cost estimates;
  • Demonstrate high product value;
  • Reliable operation with high on-line time and low maintenance;
  • Demonstrate new technology at a commercial scale.

In addition to verifying filter performance, pilot testing provides the opportunity for the operating engineer to learn to use the equipment and conduct experiments that optimize filter operation for their particular process. Pilot test trials address significant technical questions and problems prior to full-scale commercialization. The outcome of pilot plant operations verify:

  • Filtration/reaction studies verified at laboratory and pilot plant scale;
  • New technology demonstrated;
  • High volume product consistently recovered;
  • Product separation and recovery optimized;
  • Capacity testing completed;
  • Overall operating efficiency.

Media Selection 

Feasibility Case Study: Catalyst Solids Removal

A typical approach for feasibility testing and media selection is illustrated in the following test case. The objective was to evaluate the filtering characteristics of a new catalyst to support an existing LSI commercial filter installation. Filtration studies were conducted with a 70-mm disc test filter using both Grades 5 and 10 media to compare filter performance. Catalyst particle size distribution (PSD) was measured using a Horiba LA-910 Laser Scattering Particle Size Distribution Analyzer. The size range (based on volume %) was 0.51 to 60 µm with a mean size of 13.4 µm. SEM microscopy at 2000- X magnification verified particle size distribution as shown in Figure 3. Catalyst slurry was filtered once through at a constant rate using Grades 5 and 10 media housed in the 70-mm disc filter housing shown in Figure 4. A particle size distribution comparison of feed and filtrates (Grade 5) sample is shown in Figure 5. Test results indicate that filtration using Grade 5 media resulted with a lower rate of rise pressure than Grade 10 media as indicated in Figure 6. Filtrate turbidity samples were similar. Filtrate from the Grade 5 media measured 2.9 NTU, while filtrate from Grade 10 media measured 2.3 NTU. The 1/8 inch thick filter cake backwashed effectively from the Grade 5 media surface. Some catalyst remained in the porous structure of the Grade 10 media, indicating that catalyst had blocked some of the surface pores.

Test results indicate that Grade 5 media is better suited for filtration of new catalyst sample using the HyPulse LSI filter configuration. Pilot testing at the commercial facility verified results of feasibility study and resulted in purchase of replacement cartridges for an existing filter vessel.

Commercial Applications 

Application 1:

Laboratory disc tests conducted in April 1992 indicate suitability of sintered metal filter for catalyst recovery application. Bench scale pilot filter tests were conducted at the customer’s lab facility to verify filter performance and filtrate quality. In November 1992 pilot testing with continuous catalyst filtration using 2% slurry demonstrated consistent flux rates of 0.2 gpm/ft2. A comparison of filter performance from disc testing through pilot testing is listed in Table 1. Axial velocity through the filter controlled cake thickness. The rate or velocity through the filter was optimized in bench scale testing. Optimal filter performance indicated that the filter could operate at pressures < 10 PSI without backwashing. Tests were conducted over about 1500 hours with no significant change in operating performance. The project gained approval to move to the final stage.

The objective of pilot test development program was to convert isomerization process from batch to continuous. The first commercial plant was scheduled for operation in 1994. The process was started up in July 1994 in accordance with parameters established during the pilot testing. System dynamics experienced during start-up and initial operation exhibited performance similar to the pilot test studies. The filter operated successfully to recover and recycle precious metal catalyst after solvent wash and removal of 10% of the catalyst from the process after each batch. Process liquid is hazardous, however, because the filter system is completely enclosed, solvent could be used to wash and re-slurry catalyst back to the reactor.

The primary (larger) LSM catalyst filter is designed for bulk catalyst filtration and recycle. The filter design offers completely enclosed automated operation with minimal filter cleaning/regeneration. Fresh catalyst is added to each batch. The smaller LSP filter is designed for catalyst removal from the system. After 7 years of operation the filter bundle was replaced during a preventive maintenance schedule. The filtration system continues to operate since its initial installation in 1994.

Application 2:

This catalyst filtration concept was proved in laboratory testing to confirm filter operating parameters and media selection. A development program utilizing pilot testing used a reactor equipped with filtration apparatus capable of separating product from catalyst, whereby the product can be removed from the

reactor while the catalyst is retained, thus permitting the reaction to be run semi-continuously or continuously. Testing utilized the HyPulse® LSM filter design.

By equipping a reactor with a means of maintaining catalyst in the vessel, the reactant can be pumped and the catalyst free product continuously removed. The hydrogenation process stops when the catalyst charge deactivates. The preferred method of filtration was to install a re-circulation loop onto the reactor,

as shown in Figure 7. For an extended batch or continuous process, a larger charge of catalyst is used to ensure sufficiently large commercially viable production quantities. This process allows up to a 50% reduction in total cycle time and an increase in over 65% in the amount of product run as indicated in Table 2.

Application 3:

The first use of sintered metal filters using inside-out (LSI) HyPulse® filtration technology for continuous slurry oil filtration was in 1985. The installation demonstrated the suitability of sintered metal media for high temperature filtration of slurry oil for a carbon fiber development process. The filter operated reliably for many years producing clean oil with solids content of less than 20 ppm and was eventually shut down because of low product demand. Since then, refineries around the world have become aware of the benefits of filtration using sintered metal media for catalyst fines removal in slurry oil service.

Throughout the 1990’s numerous LSI filtration systems have been installed for FCC slurry oil filtration. The largest continuous filtration systems utilizes (3) 66” LSI filters as shown in the schematic in Figure 8. Filtration cycle time ranges from 2 to 16 hours operating at 30 & 60 PSI, respectively in the filtration of 1000 ppm slurry oil. Extended cycle times were obtained by running two filters simultaneously, but staggered in cycle time, with the third being on stand-by for utilization when one of the other filter units is backwashed. The filter design uses a full shell backwash. Efficiency of the recovered product using two filters on line exceeds 99.8%.

Since 1997 there have been many refineries in China have installed LSI filtration systems for catalyst removal in resid fluid catalytic cracking (RFCC) units. A filtration system with (2) 24” LSI filters was installed in a RFCC unit with 1.4 million metric tons (mt) per year capacity and an output of slurry oil of 180 mt/day. The slurry oil has an average 3,000 to 5,000 ppm solids concentration. Cycle time varies from 2 to 8 hours. The filtrate solids content is under 50 ppm. The filter is controlled by local PLC that communicates with refineries distributed control system (DCS) to enable the operator monitor the filtration in the control room. The system is running continuously since then supplying a local company with clean filtrate to produce carbon black.

Application 4:

A process for producing Uranium Dioxide utilizes a HyPulse® gas/solids venturi pulse (GSV) blowback sintered metal filters, as shown in Figure 9, for the recovery of Uranium oxide fines from a process kiln. The sintered metal filters must withstand kiln off-gas stream temperatures of 300°F and be chemically resistant to the gaseous components. The primary risks associated with this conversion are chemical and radiological. The conversion process uses strong acids and alkalis that involve turning uranium oxide into soluble forms, leading to possible inhalation of uranium. In addition, the corrosive chemicals can cause fire or explosion hazards.

Successful field applications and laboratory support provided performance data that resulted in the first commercial filter installation put in service in 1984. The completely enclosed GSV filter operates with 99.999% efficiency with a very low solids load to the filter and infrequent backpulsing. Key operating parameters include controlled approach velocity to the filter, high efficiency, and use of venturi for blowback for continuous operation. Today, one uranium conversion plant continues to operate in the United States using this patented process.

 

 

Application 5:

Cleanable sintered metal fibre filters offer an economical solution to processes with increased demand for higher particulate removal efficiency in extreme conditions. The development of metal fiber filter media such as Bekipor® contributed to an increased quality level through higher filter efficiency and a longer onstream

lifetime. Traditional separation systems such as cyclones, ElectroStatic Precipitators (ESP) and disposable filters are losing their appeal. Figure 10 compares emissions efficiency and relative cost of fiber metal compared to ESP and cyclones.

A highly porous structure, which is a characteristic of a sintered metal fibre medium, offers a high permeability and hence low pressure drop, even at high filtration velocities. This results in a low capital expenditure and low running costs. The cleanability for both on line cleaned surface filtration as for off line cleaned depth filtration is excellent.

This application used Bekiflow® HG for removal of alumina and alumina hydroxide dust having a particle size of 50% < 15 μm. Gas temperatures measured 842 °F. Dust concentration before the filter measured 250-800 mg/Nm³. Gas concentration after filtration was less than 30 mg/Nm³. Maximum pressure drop was 15 mbar. Total surface area of the filter was 830 m2. Fiber metal filters offers limited pressure drop and was tested for guaranteed lifetime of 27,000 operating hours. Customer benefits include less filter surface required, smaller bag house therefore less installation place required.

Summary 

Sintered metal media provides an effective means of filtering to remove particulate whether they are impurities or valuable by-product of a chemical process stream. These media are ideally suited for more demanding applications involving high temperatures, high pressures, and/or corrosive fluids. Chemical

companies are utilizing filtration to minimize waste products at the source rather than at the end of the line of the production process. Filtration improves product quality and protects downstream equipment in the production of chemical based products. Advances in filtration technology include the development of continuous processes to replace old batch process technology. Liquid/solids filtration using conventional leaf filters is messy and hazardous to clean and require extended re-circulation time to obtain clean product. Traditional gas/solids separation systems such as cyclones, ElectroStatic Precipitators (ESP) and disposable filters are being replaced by sintered fiber metal filtration systems.

Sintered metal filters should be operated within the design parameters to prevent premature blinding of the media due to fluctuations in process operations. Use of flow control assures the filter will not be impacted with a high flow excursion. Filter efficiency increases as the filter cake forms. The cake becomes the filter media and the porous media acts as a septum to retain the filter cake. Filter cakes can be effectively washed in-situ and backwashed from the filter housing. A gas assisted pneumatic hydropulse backwash has proven to be the most effective cleaning method for sintered porous metal filters. Sintered metal filters can be fully automated to eliminate operator exposure and lower labor costs while providing reliable, efficient operation.

 

Bekiflow and Bekipor are registered trademarks of Bekaert.

Hypulse is a registered trademark of Mott Corporation.

 

 

FAQs: Sintered Metal Technology

Q: What is sintered metal?

A: Sintered metal refers to a specialized material made by compacting and forming metal powder under heat and pressure, creating a solid, porous structure ideal for filtration and various industrial applications.

Q: How are sintered metal filters manufactured?

A: Sintered metal filters are produced by compacting metal powder in a mold and then heating it to a temperature below the metal’s melting point, causing the particles to bond without liquefying.

Q: What are the main advantages of using sintered metal filters?

A: Sintered metal filters offer high durability, excellent temperature and corrosion resistance, and the ability to withstand harsh environments, making them suitable for challenging industrial applications.

Q: In what industries are sintered metal filters commonly used?

A: Sintered metal filters are widely used across various industries, including pharmaceuticals, food and beverage, chemical processing, and aerospace, for their efficiency in removing particulates from gases and liquids.

 

Types of Sintered Filters and How To Choosing

 

 

1. What are the 4 main filter types?

1. Sintered Metal Filters

These filters are made by fusing together metal particles under heat and pressure. They can be made from different metals and alloys, each having unique properties.

  • Sintered Bronze Filter: Sintered bronze filters are known for their corrosion resistance and are often used in hydraulic systems, pneumatic systems, and other applications where a high degree of filtration is required.

  • Sintered Stainless Steel FilterSintered Stainless Steel Filter: This type offers high strength and temperature resistance, and it's often used in demanding environments like chemical processing and food and beverage applications.

  • Sintered Titanium Filter: Titanium offers excellent corrosion resistance and is suitable for use in the pharmaceutical and biotech industries.

  • Sintered Nickel Filter: Nickel sintered filters are known for their magnetic properties and are used in various industries including chemical processing and petroleum.

2. Sintered Glass Filter

Sintered glass filters are made by fusing together glass particles. They are widely used in laboratories for filtration tasks and offer a high degree of chemical resistance. They are commonly utilized in applications where precise filtration and minimal interaction with the sample are crucial.

3. Sintered Ceramic Filter

Ceramic filters are made from various ceramic materials and are known for their high-temperature resistance and stability. They are often used in the metal industry for filtering molten metal and in environmental applications to filter air or water.

4. Sintered Plastic Filter

These filters are made by fusing together plastic particles, often polyethylene or polypropylene. Sintered plastic filters are lightweight and corrosion-resistant, and they're typically used in applications where chemical compatibility and cost-effectiveness are key considerations.

In conclusion, the type of sintered filter selected depends on the specific application, considering factors such as temperature, pressure, corrosion resistance, and the nature of the substances being filtered. Different materials offer various advantages and trade-offs, so careful selection is vital to meet the required performance criteria.

 

However, if you're asking about the four main types of filters in general, they are typically categorized by their function rather than the material they are made from. Here's a general overview:

  1. Mechanical Filters: These filters remove particles from air, water, or other fluids through a physical barrier. The sintered filters you mentioned would fall into this category, as they are often used to filter particulates from gases or liquids.

  2. Chemical Filters: These filters use a chemical reaction or absorption process to remove specific substances from a fluid. For example, activated carbon filters are used to remove chlorine and other contaminants from water.

  3. Biological Filters: These filters use living organisms to remove contaminants from water or air. In a fish tank, for example, a biological filter might use bacteria to break down waste products.

  4. Thermal Filters: These filters use heat to separate substances. An example would be an oil filter in a deep fryer that uses heat to separate the oil from other substances.

The sintered filters you mentioned are specific examples of mechanical filters, and they can be made from various materials, including metal, glass, ceramic, and plastic. Different materials will offer different properties, such as resistance to corrosion, strength, and porosity, making them suitable for different applications.

 

 

2. What are sintered filters made of?

Sintered filters are made from a variety of materials, depending on their specific application and required properties. Here's a breakdown of the common materials used:

1. Sintered Metal Filters

  • Bronze: Offers good corrosion resistance.

  • Stainless Steel: Known for high strength and temperature resistance.

  • Titanium: Offers excellent corrosion resistance.

  • Nickel: Used for its magnetic properties.

2. Sintered Glass Filter

  • Glass Particles: Fused together to form a porous structure, often used in laboratory settings for precise filtration.

3. Sintered Ceramic Filter

  • Ceramic Materials: Including alumina, silicon carbide, and other compounds, used for their high-temperature resistance and stability.

4. Sintered Plastic Filter

  • Plastics such as Polyethylene or Polypropylene: These are used for their lightweight and corrosion-resistant properties.

The choice of material is guided by the specific requirements of the application, such as chemical compatibility, temperature resistance, mechanical strength, and cost considerations. Different materials provide different characteristics, making them suitable for various industrial, laboratory, or environmental uses.

 

 

3. What are the different types of sintered filters? Advantage and Disadvantage

Advantages:

  • Durability: Metal filters are robust and can withstand high pressures and temperatures.

  • Variety of Materials: Options like bronze, stainless steel, titanium, and nickel allow for customization based on application needs.

  • Reusable: Can be cleaned and reused, reducing waste.

Disadvantages:

  • Cost: Typically more expensive than plastic or glass filters.

  • Weight: Heavier than other types, which may be a consideration in some applications.

Subtypes:

  • Sintered Bronze, Stainless Steel, Titanium, Nickel: Each metal has specific advantages, such as corrosion resistance for bronze, high strength for stainless steel, and so on.

2. Sintered Glass Filter

Advantages:

  • Chemical Resistance: Resistant to most chemicals, making it suitable for laboratory applications.

  • Precision Filtration: Can achieve fine levels of filtration.

Disadvantages:

  • Fragility: More prone to breaking compared to metal or ceramic filters.

  • Limited Temperature Resistance: Not suitable for very high-temperature applications.

3. Sintered Ceramic Filter

Advantages:

  • High-Temperature Resistance: Suitable for applications involving high temperatures, such as molten metal filtration.

  • Chemical Stability: Resistant to corrosion and chemical attack.

Disadvantages:

  • Brittleness: Can be prone to cracking or breaking if mishandled.

  • Cost: Can be more expensive than plastic filters.

4. Sintered Plastic Filter

Advantages:

  • Lightweight: Easier to handle and install.

  • Corrosion-Resistant: Suitable for applications involving corrosive chemicals.

  • Cost-Effective: Generally more affordable than metal or ceramic filters.

Disadvantages:

  • Lower Temperature Resistance: Not suitable for high-temperature applications.

  • Less Robust: May not withstand high pressures or mechanical stress as well as metal filters.

In conclusion, the selection of a sintered filter depends on various factors, such as the filtration requirements, operating conditions (temperature, pressure, etc.), chemical compatibility, and budget constraints. Understanding the advantages and disadvantages of each type of sintered filter allows for an informed choice that best fits the specific application.

 

 

4. What is a sintered filter used for?

A sintered filter is used in a wide variety of applications across different industries due to its unique properties, including controlled porosity, strength, and chemical resistance. Here's an overview of the common uses for sintered filters:

1. Industrial Filtration

  • Chemical Processing: Removal of impurities from chemicals and liquids.

  • Oil and Gas: Separation of particles from fuels, oils, and gases.

  • Food and Beverage Industry: Ensuring purity and sanitation in processing.

  • Pharmaceutical Manufacturing: Filtering contaminants from pharmaceutical products.

2. Laboratory Applications

  • Analytical Testing: Providing precise filtration for various laboratory tests and experiments.

  • Sample Preparation: Preparing samples by removing unwanted particles or debris.

3. Environmental Protection

  • Water Treatment: Filtering impurities from drinking water or wastewater.

  • Air Filtration: Removing pollutants and particles from the air.

4. Automotive and Transportation

  • Hydraulic Systems: Protecting components by filtering out contaminants in hydraulic fluids.

  • Fuel Filtration: Ensuring clean fuel for efficient engine performance.

5. Medical and Healthcare

  • Medical Devices: Utilized in devices like ventilators and anesthesia machines for clean airflow.

  • Sterilization: Ensuring the purity of gases and liquids in medical applications.

6. Electronics Manufacturing

  • Gas Purification: Providing clean gases used in semiconductor manufacturing.

7. Metal Industry

  • Molten Metal Filtration: Filtering impurities from molten metals during casting processes.

8. Aerospace

  • Fuel and Hydraulic Systems: Ensuring cleanliness and performance in aerospace applications.

The choice of sintered filter, including the material and design, is guided by the specific requirements of the application, such as filtration size, temperature, chemical compatibility, and pressure resistance. Whether it's ensuring the purity of food and water, enhancing industrial processes, or supporting critical healthcare and transportation functions, sintered filters play a vital role in numerous sectors.

 

 

5. How are sintered metal filters made?

Sintered metal filters are made through a process known as sintering, which involves the use of heat and pressure to fuse metal particles into a cohesive, porous structure. Here's a step-by-step explanation of how sintered metal filters are typically made:

1. Material Selection:

  • The process begins by selecting the appropriate metal or metal alloy, such as stainless steel, bronze, titanium, or nickel, depending on the specific application and required properties.

2. Powder Preparation:

  • The selected metal is ground into a fine powder, usually through mechanical milling or atomization.

3. Blending and Mixing:

  • The metal powder may be blended with additives or other materials to achieve specific characteristics, such as enhanced strength or controlled porosity.

4. Shaping:

  • The blended powder is then shaped into the desired form of the filter. This can be done through various methods like pressing, extrusion, or injection molding.

  • In the case of pressing, a mold of the desired filter shape is filled with the powder, and a uniaxial or isostatic press is used to compact the powder into the desired shape.

5. Pre-Sintering (Optional):

  • Some processes may include a pre-sintering step at a lower temperature to remove any organic binders or other volatile substances before the final sintering.

6. Sintering:

  • The shaped part is heated to a temperature below the melting point of the metal but high enough to cause the particles to bond together.

  • This process is usually conducted in a controlled atmosphere to prevent oxidation and contamination.

  • The temperature, pressure, and time are carefully controlled to achieve the desired porosity, strength, and other properties.

7. Post-Processing:

  • After sintering, additional processes like machining, grinding, or heat treatment may be applied to achieve the final dimensions, surface finish, or specific mechanical properties.

  • If required, the filter may be cleaned to remove any residues or impurities from the manufacturing process.

8. Quality Control and Inspection:

  • The final filter is inspected and tested to ensure that it meets the required specifications and standards for the application.

Sintered metal filters are highly customizable, allowing for control over properties like pore size, shape, mechanical strength, and chemical resistance. This makes them suitable for a wide range of demanding filtration applications across various industries.

 

6. What filtration system is most effective?

Determining the "most effective" filtration system depends on the specific requirements of the application, including the type of substance being filtered (e.g., air, water, oil), the desired purity level, operating conditions, budget, and regulatory considerations. Below are some common filtration systems, each with its own set of advantages and suitability for various applications:

1. Reverse Osmosis (RO) Filtration

  • Best For: Water purification, especially for desalination or removal of small contaminants.

  • Advantages: Highly effective at removing salts, ions, and small molecules.

  • Disadvantages: High energy consumption and potential loss of beneficial minerals.

2. Activated Carbon Filtration

  • Best For: Removal of organic compounds, chlorine, and odors in water and air.

  • Advantages: Effective at improving taste and smell, readily available.

  • Disadvantages: Not effective against heavy metals or microorganisms.

3. Ultraviolet (UV) Filtration

  • Best For: Disinfection of water by killing or inactivating microorganisms.

  • Advantages: Chemical-free and highly effective against pathogens.

  • Disadvantages: Does not remove non-living contaminants.

4. High-Efficiency Particulate Air (HEPA) Filtration

  • Best For: Air filtration in homes, healthcare facilities, and cleanrooms.

  • Advantages: Captures 99.97% of particles as small as 0.3 microns.

  • Disadvantages: Does not remove odors or gases.

5. Sintered Filtration

  • Best For: Industrial applications requiring high-temperature resistance and precise filtration.

  • Advantages: Customizable pore sizes, reusable, and suitable for aggressive media.

  • Disadvantages: Potentially higher costs compared to other methods.

6. Ceramic Filtration

  • Best For: Water purification in areas with limited resources.

  • Advantages: Effective at removing bacteria and turbidity, low-cost.

  • Disadvantages: Slower flow rates, may require frequent cleaning.

7. Bag or Cartridge Filtration

  • Best For: General industrial liquid filtration.

  • Advantages: Simple design, easy to maintain, various material options.

  • Disadvantages: Limited filtration capacity, may require frequent replacement.

In conclusion, the most effective filtration system is highly dependent on the specific application, contaminants targeted, operational requirements, and budget considerations. Often, a combination of filtration technologies may be employed to achieve the desired results. Consulting with filtration experts and conducting a proper assessment of the specific needs can guide the selection of the most suitable and effective filtration system.

 

7. What is the type of filter that are commonly used?

There are several types of filters commonly used across various fields and applications. Here are some of the most common types:

  1. Low-Pass Filter: This type of filter allows low-frequency signals to pass through while attenuating high-frequency signals. It's often used to eliminate noise or unwanted high-frequency components from a signal.

  2. High-Pass Filter: High-pass filters allow high-frequency signals to pass while attenuating low-frequency signals. They're used to remove low-frequency noise or DC offset from a signal.

  3. Band-Pass Filter: A band-pass filter allows a certain range of frequencies, called the passband, to pass through while attenuating frequencies outside that range. It's useful for isolating a specific frequency range of interest.

  4. Band-Stop Filter (Notch Filter): Also known as a notch filter, this type of filter attenuates a specific range of frequencies while allowing frequencies outside that range to pass. It's commonly used to eliminate interference from specific frequencies.

  5. Butterworth Filter: This is a type of analog electronic filter that provides a flat frequency response in the passband. It's commonly used in audio applications and signal processing.

  6. Chebyshev Filter: Similar to the Butterworth filter, the Chebyshev filter provides a steeper roll-off between the passband and the stopband, but with some ripple in the passband.

  7. Elliptic Filter (Cauer Filter): This type of filter offers the steepest roll-off between the passband and the stopband but allows for ripple in both regions. It's used when a sharp transition between passband and stopband is needed.

  8. FIR Filter (Finite Impulse Response): FIR filters are digital filters with a finite response duration. They're often used for linear phase filtering and can have both symmetric and asymmetric responses.

  9. IIR Filter (Infinite Impulse Response): IIR filters are digital or analog filters with feedback. They can provide more efficient designs but may introduce phase shifts.

  10. Kalman Filter: A recursive mathematical algorithm used for filtering and predicting future states based on noisy measurements. It's widely used in control systems and sensor fusion applications.

  11. Wiener Filter: A filter used for signal restoration, noise reduction, and image deblurring. It aims to minimize the mean square error between the original and filtered signals.

  12. Median Filter: Used for image processing, this filter replaces each pixel's value with the median value from its neighborhood. It's effective in reducing impulse noise.

These are just a few examples of the many types of filters used in various fields such as signal processing, electronics, telecommunications, image processing, and more. The choice of filter depends on the specific application and the desired characteristics of the filtered output.

 

 

8. ALL Sintered Filter Be Porous ? 

Yes, sintered filters are characterized by their porous nature. Sintering is a process that involves heating and compressing a powdered material, such as metal, ceramic, or plastic, without melting it completely. This results in a solid structure that contains interconnected pores throughout the material.

The porosity of a sintered filter can be carefully controlled during the manufacturing process by adjusting factors such as the particle size of the material, sintering temperature, pressure, and time. The resulting porous structure allows the filter to selectively pass fluids or gases while trapping and removing unwanted particles and contaminants.

The size, shape, and distribution of the pores in a sintered filter can be tailored to meet specific filtration requirements, such as the desired filtration efficiency and flow rate. This makes sintered filters highly versatile and suitable for a wide range of applications, including industrial, chemical, water, and air filtration systems. The ability to control the porosity allows sintered filters to be used for both coarse and fine filtration, depending on the needs of the application.

 

 

9. How to Choose Right Sintered Filters for your Filtration System ?

Choosing the right sintered filters for your filtration system is a critical task that requires careful consideration of various factors. Here's a guide to help you make an informed decision:

1. Identify the Filtration Requirements

  • Contaminants: Determine the type and size of particles or contaminants that need to be filtered.

  • Filtration Efficiency: Decide the level of filtration required (e.g., removing 99% of particles above a certain size).

2. Understand the Operating Conditions

  • Temperature: Choose materials that can withstand the operating temperatures of the system.

  • Pressure: Consider the pressure requirements, as sintered filters must be strong enough to endure the operating pressure.

  • Chemical Compatibility: Select materials that are resistant to any chemicals present in the substances being filtered.

3. Choose the Right Material

  • Sintered Metal Filters: Select from materials like stainless steel, bronze, titanium, or nickel based on the specific needs.

  • Sintered Ceramic or Plastic Filters: Consider these if they meet your temperature, pressure, and chemical resistance requirements.

4. Determine the Pore Size and Structure

  • Pore Size: Choose the pore size based on the smallest particles that need to be filtered.

  • Pore Structure: Consider whether uniform pore sizes or a gradient structure is required for your application.

5. Consider the Flow Rate

  • Evaluate the flow rate requirements of the system and choose a filter with the appropriate permeability to handle the desired flow.

6. Evaluate Cost and Availability

  • Consider the budget constraints and select a filter that offers the required performance at an acceptable cost.

  • Think about the availability and lead time for custom or specialized filters.

7. Compliance and Standards

  • Ensure the selected filter meets any relevant industry standards or regulations specific to your application.

8. Maintenance and Lifecycle Considerations

  • Consider how often the filter will need to be cleaned or replaced and how this fits with maintenance schedules.

  • Think about the expected lifespan of the filter in your specific operating conditions.

9. Consult with Experts or Suppliers

  • If unsure, engage with filtration experts or suppliers who can assist in selecting the right filter for your specific application.

By thoroughly understanding the specific requirements of your system and carefully considering the factors above, you can select the right sintered filter that will deliver the performance, reliability, and efficiency required for your filtration system.

 

Are you looking for the perfect filtration solution tailored to your specific needs?

HENGKO‘s experts specialize in providing top-notch, innovative filtration products designed to meet a wide range of applications.

Don't hesitate to reach out to us with any questions or to discuss your unique requirements.

Contact us today at ka@hengko.com, and let's take the first step towards optimizing your filtration system.

Your satisfaction is our priority, and we're eager to assist you with the best solutions available! 

 

 

Post time: Aug-09-2023
Post time: Aug-09-2023

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